ChemInform Abstract: Single-Crystal Structure Determination and Spectroscopic Characterization of KSr4(BO3)3.

ChemInform ◽  
2013 ◽  
Vol 44 (28) ◽  
pp. no-no
Author(s):  
Gerhard Sohr ◽  
Doris Clara ◽  
Hubert Huppertz
2013 ◽  
Vol 68 (4) ◽  
pp. 338-344 ◽  
Author(s):  
Gerhard Sohr ◽  
Doris Clara ◽  
Hubert Huppertz

During attempts to synthesize a high-pressure phase of KSr4(BO3)3 using pressures of up to 12 GPa, single crystals of the normal-pressure phase KSr4(BO3)3 with sufficient quality for singlecrystal diffraction experiments could be obtained at 3 GPa and 1300 °C in a Walker-type multianvil apparatus. The single-crystal structure determination verified the published powder diffraction data of KSr4(BO3)3 revealing the non-centrosymmetric space group Ama2 with a = 1104:8(2), b=1199:1(2), c=688:8(2) pm and Z =4. Additionally, IR- and Raman-spectroscopic investigations were performed on single crystals of the compound.


Author(s):  
P. Ballirano ◽  
R. Caminiti ◽  
C. Sadun ◽  
V. M. Coiro ◽  
G. Mancini ◽  
...  

AbstractThe structures of cetylpyridiniumammonium bromide (CPyB) and cetylquinuclidinium bromide (CQB), two tetraalkylammonium bromide surfactants, are reported. In particular, whereas the structure solution of CPyB was carried out through conventional single-crystal diffractometry, the structure of CQB has been determined by means of powder diffractometry. CPyB crystallizes in


CrystEngComm ◽  
2021 ◽  
Author(s):  
Brendan F. Abrahams ◽  
Christopher J. Commons ◽  
Timothy A. Hudson ◽  
Robin W. Sanchez Arlt

The chance discovery of crystals of calcium acetate hemihydrate, which is commonly formed on calcareous heritage objects, has allowed its single crystal structure determination; this remarkable crystal structure consists of chiral rod-like units.


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