Single-crystal Structure Determination and Spectroscopic Characterization of KSr4(BO3)3
2013 ◽
Vol 68
(4)
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pp. 338-344
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Keyword(s):
During attempts to synthesize a high-pressure phase of KSr4(BO3)3 using pressures of up to 12 GPa, single crystals of the normal-pressure phase KSr4(BO3)3 with sufficient quality for singlecrystal diffraction experiments could be obtained at 3 GPa and 1300 °C in a Walker-type multianvil apparatus. The single-crystal structure determination verified the published powder diffraction data of KSr4(BO3)3 revealing the non-centrosymmetric space group Ama2 with a = 1104:8(2), b=1199:1(2), c=688:8(2) pm and Z =4. Additionally, IR- and Raman-spectroscopic investigations were performed on single crystals of the compound.
2017 ◽
Vol 232
(7-9)
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1991 ◽
Vol 168
(2)
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pp. 377-382
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1998 ◽
Vol 213
(2)
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2010 ◽
Vol 66
(a1)
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pp. s317-s317
2011 ◽
Vol 17
(46)
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pp. 12928-12931
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2016 ◽
Vol 2016
(20)
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pp. 3292-3298
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