Low Temperature Synthesis and Characterization of Li1.2-yNayV3O8 (0 ≤ y ≤ 1.2) from V2O5 Gel

2010 ◽  
Vol 21 (3) ◽  
pp. 232-237
Author(s):  
Xie Jing-Gang ◽  
Xiao Jle ◽  
Zhan Hui ◽  
Zhou Yun-Hong
2007 ◽  
Vol 5 (1) ◽  
pp. 169-176 ◽  
Author(s):  
Abdülhadi Baykal ◽  
Yüksel Köseoğlu ◽  
Mehmet Şenel

AbstractHeating hydrous manganese (II) hydroxide gel at 85 °C for 12 hours produces Mn3O4 nanoparticles. They were characterized by X-ray powder diffraction (XRD) and infrared spectroscopy (FTIR). The particle size estimated from the SEM and X-ray peak broadening is approximately 32 nm, showing them to be nanocrystalline. EPR measurements confirm a typical Mn2+signal with a highly resolved hyperfine structure.


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