New method for the synthesis of macrocyclic compounds Communication 4. Effect of the length of the aliphatic chain on the character and yields of the products formed in the intramolecular acylation of 2-thiophenealkanoyl chlorides

1963 ◽  
Vol 12 (8) ◽  
pp. 1320-1327 ◽  
Author(s):  
Ya. L. Gol'dfarb ◽  
S. Z. Taits ◽  
L. I. Belen'kii
Keyword(s):  
New Method ◽  
Aliphatic Chain ◽  
Macrocyclic Compounds

New method for the synthesis of macrocyclic compounds

1972 ◽  
Vol 8 (2) ◽  
pp. 149-155 ◽  
Author(s):  
S. Z. Taits ◽  
O. A. Kalinovskii ◽  
V. S. Bogdanov ◽  
Ya. L. Gol'dfarb
Keyword(s):  
New Method ◽  
Macrocyclic Compounds

New method of synthesis of macrocyclic compounds

1970 ◽  
Vol 19 (10) ◽  
pp. 2189-2194 ◽  
Author(s):  
O. A. Kalinovskii ◽  
S. Z. Taits ◽  
Ya. L. Gol'dfarb
Keyword(s):  
New Method ◽  
Macrocyclic Compounds

A new method of synthesizing macrocyclic compounds

1968 ◽  
Vol 17 (4) ◽  
pp. 735-740 ◽  
Author(s):  
S. Z. Taits ◽  
�. A. Krasnyanskaya ◽  
Ya. L. Gol'dfarb
Keyword(s):  
New Method ◽  
Macrocyclic Compounds

A new method of syntheses of 18-membered macrocyclic diphenyltin(IV) compounds and crystal structures of {Ph2Sn[S(C6H3NO)O]}3·Y (Y = 2H2O or 4C6H6) and {Ph3Sn[S(C6H3NO)O]SnPh3(EtOH)}·[EtOH]

2004 ◽  
Vol 82 (5) ◽  
pp. 608-615 ◽  
Author(s):  
Chunlin Ma ◽  
Qin Jiang ◽  
Rufen Zhang
Keyword(s):  
Crystal Structure ◽  
Crystal Structures ◽  
New Method ◽  
Macrocyclic Compounds ◽  
X Ray ◽  
Stacking Interaction ◽  
Π Stacking ◽  
Triphenyltin Chloride ◽  
Π Stacking Interaction ◽  
Solvent Molecules

Two diphenyltin(IV) compounds: {Ph2Sn[S(C6H3NO)O]}3·Y (Y = 2H2O, 1; 4C6H6, 2) have been unexpectedly obtained by the reactions of triphenyltin chloride with 2-mercaptonicotinic acid in the presence of Et3N. However, by the reaction of the same reactants in the presence of EtONa, only a new triphenyltin(IV) compound ({Ph3Sn[S(C6H3NO)O]SnPh3(EtOH)}·[EtOH], 3) was obtained. The X-ray analyses reveal that compounds 1 and 2 are trinuclear, 18-membered macrocyclic compounds while 3 is a dinuclear compound. Specially, π-π stacking interaction was recognized in crystals of compound 1, which makes it a dimer. Co-crystallization was found in the crystals of all the three compounds 1, 2, and 3, the co-crystallized solvent molecules are water, benzene, and ethanol molecules, respectively. A possible dephenylation mechanism of 1 and 2 was illustrated in detail.Key words: triphenyltin, 2-mercaptonicotinic acid, dephenylation, macrocyclic, π-π stacking interaction, co-crystallization, crystal structure.

New method for the synthesis of macrocyclic compounds

1968 ◽  
Vol 17 (3) ◽  
pp. 555-558
Author(s):  
S. Z. Taits ◽  
F. D. Alashev ◽  
Ya. L. Gol'dfarb
Keyword(s):  
New Method ◽  
Macrocyclic Compounds

New method for the synthesis of macrocyclic compounds

1973 ◽  
Vol 9 (1) ◽  
pp. 13-17 ◽  
Author(s):  
S. Z. Taits ◽  
V. N. Bulgakova ◽  
Ya. L. Gol'dfarb
Keyword(s):  
New Method ◽  
Macrocyclic Compounds

New method for the synthesis of macrocyclic compounds

1973 ◽  
Vol 9 (5) ◽  
pp. 576-582 ◽  
Author(s):  
S. Z. Taits ◽  
O. A. Kalinovskii ◽  
B. V. Lopatin ◽  
Ya. L. Gol'dfarb
Keyword(s):  
New Method ◽  
Macrocyclic Compounds
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