Instrumental neutron activation analysis in geochemistry: Emphasis on spectral and uranium fission product interferences

2005 ◽  
Vol 265 (3) ◽  
pp. 511-514 ◽  
Author(s):  
M. D. A. Tshiashala
2013 ◽  
Vol 101 (9) ◽  
pp. 601-606
Author(s):  
M. Wasim

Summary Miniature neutron source reactors (MNSR) are known for their stable neutron flux characteristics and are mostly employed for neutron activation analysis (NAA). Interfering reactions are sometimes observed in instrumental neutron activation analysis (INAA). Failure to correct for these interferences produces significant systematic positive errors. This paper provides correction factors for the interferences caused by the threshold reactions and fission products of 235U. These factors were calculated by using the experimentally determined thermal, epithermal and fast neutron flux and epithermal neutron flux shape factor and the nuclear data from the literature using the Høgdahl convention. Correction factors were calculated for (n, p) and (n, α) reactions for the most commonly observed radionuclides in INAA. Similarly, correction factors for uranium fission were calculated for 9 elements (Ce, Ba, La, Mo, Nd, Pd, Ru, Sm and Zr). The correction factors were validated by analyzing different materials. A comparison of uranium fission factors with those published in the literature showed a good agreement except for 97Zr, 99Mo and 131Ba which is due to difference in the flux characteristics. In general, these factors can be used with confidence.


2016 ◽  
Vol 5 (03) ◽  
pp. 4892 ◽  
Author(s):  
Ratna Raju M.* ◽  
Madhusudhana Rao P. V. ◽  
Seshi Reddy T. ◽  
Raju M. K. ◽  
Brahmaji Rao J. S. ◽  
...  

A study was undertaken to evaluate the inorganic elements for humans in two Indian medicinal plants leaves, namely Sphaeranthus indicus, and Cassia fistula by Instrumental Neutron Activation Analysis (INAA). INAA experiment was performed by using 20 kW KAMINI Reactor at Indira Gandhi Centre for Atomic Research (IGCAR), Kalpakkam. The emitted gamma rays were measured using gamma ray spectrometer. The concentrations of Al, Br, Ca, Fe, K, La, Mg, Mn, Na, Sc, V and Zn were determined in the selected medicinal plants. The medicinal leaves are using in treatment of various important ailments. The elemental content in selected medicinal leaves is various proportions depending on the soil composition, location of plant specimen and the climate in which the plant grows.


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