Diastereoselective synthesis of ethyl (Z)-3-(8-methylimidazo-[1,2-a]pyrid-2-yl)-2-phenylthioacrylate. X-ray crystal structure and conformational analysis

1995 ◽  
Vol 355 (2) ◽  
pp. 177-183 ◽  
Author(s):  
A Gautier ◽  
D Roche ◽  
J Métin ◽  
A Carpy ◽  
M Madesclaire
1996 ◽  
Vol 35 (6) ◽  
pp. 1647-1652 ◽  
Author(s):  
Guy Schröder ◽  
Jirí Kozelka ◽  
Michal Sabat ◽  
Marie-Hélène Fouchet ◽  
Rut Beyerle-Pfnür ◽  
...  

2003 ◽  
Vol 51 (6) ◽  
pp. 688-696 ◽  
Author(s):  
Fumikazu Ito ◽  
Tetsuya Moriguchi ◽  
Yasuyuki Yoshitake ◽  
Masashi Eto ◽  
Shoji Yahara ◽  
...  

Synlett ◽  
2021 ◽  
Author(s):  
Hong-Wu Zhao ◽  
Heng Zhang ◽  
Lu-Yu Cai ◽  
Zhe Tang ◽  
Xiao-Zu Fan ◽  
...  

Promoted by K2CO3 (2.0 equiv), the 1,3-dipolar [3+3] cycloaddition between 1, 4-benzodiazepinone-based nitrones and α-halohydroxamates processed smoothly under the mild reaction conditions and delivered structurally novel and complex cis or trans-configured d-edge-heterocycle-fused 1,4-benzodiazepinones in up to >99% isolated yield with >20:1 dr. The relative configuration of the title chemical entities was clearly identified with the use of X-ray single crystal structure analysis. The reaction mechanism was assumed to interpret the diastereoselective production of the obtained cis or trans-configured d-edge-heterocycle-fused 1, 4-benzodiazepinones.


1987 ◽  
Vol 320 (2) ◽  
pp. C19-C22 ◽  
Author(s):  
Stephen G. Davies ◽  
Isabelle M. Dordor-Hedgecock ◽  
Kevin H. Sutton ◽  
Mark Whittaker

1985 ◽  
Vol 107 (24) ◽  
pp. 6950-6956 ◽  
Author(s):  
Fathieh Shafiee ◽  
James R. Damewood ◽  
Kenneth J. Haller ◽  
Robert West

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