Microscopical and physical characterization of microwave and microwave-hydrothermal synthesis products

Micron ◽  
2013 ◽  
Vol 44 ◽  
pp. 21-44 ◽  
Author(s):  
X.H. Zhu ◽  
Q.M. Hang
Keyword(s):  
Hydrothermal Synthesis ◽  
Physical Characterization ◽  
Microwave Hydrothermal

Microwave-Hydrothermal Synthesis and Structural Characterization of Multiferroic Bismuth Ferrite Nanostructures

2010 ◽  
Vol 409 (1) ◽  
pp. 204-210 ◽  
Author(s):  
Xinhua Zhu ◽  
Yun Yang ◽  
Kai He ◽  
Jianmin Zhu ◽  
Song Ye ◽  
...  
Keyword(s):  
Hydrothermal Synthesis ◽  
Structural Characterization ◽  
Bismuth Ferrite ◽  
Microwave Hydrothermal

Microwave-hydrothermal synthesis and characterization of Co-VSB-5 microporous framework

2007 ◽  
Vol 15 (3) ◽  
pp. 271-276 ◽  
Author(s):  
Bharat L. Newalkar ◽  
T. Chiranjeevi ◽  
N. V. Choudary ◽  
S. Komarneni
Keyword(s):  
Hydrothermal Synthesis ◽  
Synthesis And Characterization ◽  
Microwave Hydrothermal

Hydrothermal Synthesis of Vanadium Oxides

1996 ◽  
Vol 453 ◽  
Author(s):  
Thomas Chirayil ◽  
Peter Zavalij ◽  
M. Stanley Whittingham
Keyword(s):  
Acetic Acid ◽  
Hydrothermal Synthesis ◽  
Critical Factor ◽  
Vanadium Oxides ◽  
Synthesis And Characterization ◽  
Cluster Compound ◽  
Soft Chemistry ◽  
Microwave Hydrothermal ◽  
Reaction Media

AbstractThe pH of the reaction media is a critical factor in the formation of new vanadium oxides with the tetramethylammonium (TMA) ion via the conventional hydrothermal method. New vanadium oxides; TMAV3O7, Li0.6V2−δO4−δ·H2O and Li0.6V2−δO4−δ, TMAV4O10, and two more new vanadium phases with d spacings of 11.5Å and 19.1Å are formed as the pH is varied with acetic acid. The synthesis and characterization of TMAV3O7, a new vanadium oxide with tetramethylammonium ions residing between its layers is discussed. The intercalation of alkylamines, DMSO, and water into Li0.6V2−δO4−δ·H2O is described. Microwave hydrothermal synthesis is a new and alternate soft chemistry technique used to accelerate the synthesis of TMAV4O10. This method also aided in the formation of a new cluster compound, [Li(H2O)4]2TMA(V10O28)·4H2O.

Structural Characterization of Zirconia Nanoparticles Prepared by Microwave-Hydrothermal Synthesis

2009 ◽  
Vol 30 (10) ◽  
pp. 1511-1516 ◽  
Author(s):  
A. Rizzuti ◽  
C. Leonelli ◽  
A. Corradi ◽  
E. Caponetti ◽  
D. Chillura Martino ◽  
...  
Keyword(s):  
Hydrothermal Synthesis ◽  
Structural Characterization ◽  
Microwave Hydrothermal ◽  
Zirconia Nanoparticles
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