Determination of trace iodide in iodised table salt on silver sulfate-modified carbon paste electrode by differential pulse voltammetry with electrochemical solid phase nano-extraction

Talanta ◽  
2010 ◽  
Vol 80 (3) ◽  
pp. 1234-1238 ◽  
Author(s):  
Yongchun Zhu ◽  
Jingjing Guan ◽  
Lu Cao ◽  
Jie Hao
The Analyst ◽  
1988 ◽  
Vol 113 (11) ◽  
pp. 1719-1722 ◽  
Author(s):  
Lucas Hernández ◽  
Pedro Hernández ◽  
Manuel H. Blanco ◽  
Encarnacion Lorenzo ◽  
Engracia Alda

2020 ◽  
Vol 16 (8) ◽  
pp. 1063-1070
Author(s):  
Lin Zhang ◽  
Xiaojing Si ◽  
Xiaoxia Yan ◽  
Haibo He ◽  
Dongmei Deng ◽  
...  

Background: Paracetamol is a common antipyretic and analgesic drug, but its excessive intake can accumulate toxic metabolites and cause kidney and liver damage, so it is critical to determine the content of paracetamol for clinical diagnosis and dose use. Methods: Au-reduced graphene oxide (Au-rGO) nanocomposite decorated with poly(L-cysteine) on carbon paste electrode was fabricated for the determination of paracetamol. Au-rGO was first coelectrodeposited on the carbon paste electrode surface. Afterwards, L-cysteine was electropolymerized to fabricate the Au-rGO/poly(L-cysteine) modified carbon paste electrode. Scanning electron microscope was used to characterize the morphology of Au-rGO and poly(L-cysteine)/Au-rGO. The electrochemical properties of the sensor were studied by cyclic voltammetry and differential pulse voltammetry. Results: After exploring the optimal conditions, the sensor showed a wide linear response for paracetamol detection in the range of 1-200 μM with a detection limit of 0.5 μM (S/N = 3). Conclusion: The fabricated sensor demonstrated good sensitivity with rapid detection capacity in real samples.


2019 ◽  
Vol 84 (2) ◽  
pp. 175-185 ◽  
Author(s):  
Mohadeseh Safaei ◽  
Hadi Beitollahi ◽  
Masoud Shishehbore ◽  
Somayeh Tajik ◽  
Rahman Hosseinzadeh

A carbon paste electrode (CPE) was modified with N-(ferrocenylmethylidene) fluorene-2-amine and graphene/ZnO nanocomposite. The electrooxidation of captopril (CAP) at the surface of the modified electrode was studied using electrochemical approaches. The electrochemical study of the modified electrode, as well as its efficiency for the electrocatalytic oxidation of captopril, is described. The electrode was used to study the electrocatalytic oxidation of captopril, by cyclic voltammetry (CV), chronoamperometry (CHA) and differential pulse voltammetry (DPV) as diagnostic techniques. It has been found that the oxidation of captopril at the surface of modified electrode occurs at a potential of about 340 mV less positive than that of an unmodified CPE. DPV of captopril at the electrochemical sensor exhibited two linear dynamic ranges (0.1?100.0 and 100.0?800.0 ?M) with a detection limit (3?) of 0.05 ?M.


2021 ◽  
Author(s):  
Priscila Azevedo Liberato ◽  
Leonardo Luiz Luiz Okumura ◽  
Astréa Filomena de Souza Silva ◽  
Herbert Aleixo ◽  
Júnio Gonçalves Silva ◽  
...  

A new methodology to determine direct the fungicide Boscalid (BSC) was developed and successfully applied in red grape 100% juice, peel extracts, pulp and purple grape seed (Vitis labrusca L.)...


Sign in / Sign up

Export Citation Format

Share Document