The determination of sub-microgram quantities of arsenic by radioactivation. Part III. The determination of arsenic in biological material

The Analyst ◽  
1952 ◽  
Vol 77 (913) ◽  
pp. 196 ◽  
Author(s):  
A. A. Smales ◽  
B. D. Pate
Keyword(s):  
Biological Material

Determination of platinum in biological material by differential pulse polarography: Analysis in urine, plasma and tissue following sample combustion

1983 ◽  
Vol 48 (10) ◽  
pp. 2903-2908 ◽  
Author(s):  
Viktor Vrabec ◽  
Oldřich Vrána ◽  
Vladimír Kleinwächter
Keyword(s):  
Biological Material ◽  
Biological Fluid ◽  
Mercury Electrode ◽  
Differential Pulse ◽  
Differential Pulse Polarography ◽  
Linear Calibration ◽  
Catalytic Current ◽  
Pulse Polarography ◽  
Dropping Mercury Electrode

A method is described for determining total platinum content in urine, blood plasma and tissues of patients or experimental animals receiving cis-dichlorodiamineplatinum(II). The method is based on drying and combustion of the biological material in a muffle furnace. The product of the combustion is dissolved successively in aqua regia, hydrochloric acid and ethylenediamine. The resulting platinum-ethylenediamine complex yields a catalytic current at a dropping mercury electrode allowing to determine platinum by differential pulse polarography. Platinum levels of c. 50-1 000 ng per ml of the biological fluid or per 0.5 g of a tissue can readily be analyzed with a linear calibration.

scholarly journals THE DETERMINATION OF IODINE IN BIOLOGICAL MATERIAL

1935 ◽  
Vol 110 (1) ◽  
pp. 29-38
Author(s):  
Virginia Trevorrow ◽  
Gladys J. Fashena
Keyword(s):  
Biological Material
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