Synthesis and characterization of PEDSCD and its application as a flame retardant in epoxy resins

In this study, a highly effective flame retardant agent, called polybicyclopentaerythritol phosphate-O-4-imino-p-phenylmethane-4-imino-2-chloro-1,3,5-s-triazine (PEDMCD), has been prepared through a direct polycondensation reaction.

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Synthesis and characterization of SPDSCD and its flame retardant application on epoxy resins

RSC Advances ◽

10.1039/d0ra05167e ◽

2020 ◽

Vol 10 (48) ◽

pp. 28654-28663

Author(s):

Yi Zhang ◽

Weiwei Yang ◽

Wei Zhao ◽

Fang Ruan ◽

Shulei Li ◽

...

Keyword(s):

Flame Retardant ◽

Epoxy Resins ◽

Synthesis And Characterization ◽

Direct Polycondensation ◽

Polycondensation Reaction

In this study, a flame retardant agent, 2,4,8,10-tetraoxo-3,9-diphosphospiro[5.5]undecane spirophosphate-4,4-diaminopair benzene disulfone-1,3,5-himetriazine (SPDSCD), is synthesized through a direct polycondensation reaction.

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The synthesis and characterization of a novel phosphorus-nitrogen containing flame retardant and its application in epoxy resins

Journal of Applied Polymer Science ◽

10.1002/app.41079 ◽

2014 ◽

Vol 131 (22) ◽

pp. n/a-n/a ◽

Cited By ~ 15

Author(s):

Geyun You ◽

Zhiquan Cheng ◽

Hao Peng ◽

Hongwu He

Keyword(s):

Flame Retardant ◽

Epoxy Resins ◽

Synthesis And Characterization

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Synthesis and characterization of phosphorus- and silicon-containing flame-retardant curing agents and a study of their effect on thermal properties of epoxy resins

Journal of Coatings Technology and Research ◽

10.1007/s11998-014-9579-6 ◽

2014 ◽

Vol 11 (4) ◽

pp. 631-637 ◽

Cited By ~ 11

Author(s):

Seema Agrawal ◽

Anudeep Kumar Narula

Keyword(s):

Thermal Properties ◽

Flame Retardant ◽

Epoxy Resins ◽

Synthesis And Characterization ◽

Curing Agents

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Synthesis and characterization of functional eugenol derivative based layered double hydroxide and its use as a nanoflame-retardant in epoxy resin

Journal of Materials Chemistry A ◽

10.1039/c4ta05740f ◽

2015 ◽

Vol 3 (7) ◽

pp. 3471-3479 ◽

Cited By ~ 69

Author(s):

Cheng Li ◽

Jintao Wan ◽

Ehsan Naderi Kalali ◽

Hong Fan ◽

De-Yi Wang

Keyword(s):

Flame Retardant ◽

Epoxy Resin ◽

Layered Double Hydroxide ◽

Epoxy Resins ◽

Synthesis And Characterization ◽

Double Hydroxide

Aiming to develop a multi-functional flame retardant for epoxy resins, a novel bio-based eugenol derivative (SIEPDP) was synthesized, and was used to modify Mg–Al layered double hydroxide (SIEPDP-LDH). This modified SIEPDP-LDH was used as a novel nanoflame-retardant for bisphenol epoxy resins and compared with unmodified pristine LDH.

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Synthesis and characterization of a DOPO-substitued organophosphorus oligomer and its application in flame retardant epoxy resins

Progress in Organic Coatings ◽

10.1016/j.porgcoat.2010.12.013 ◽

2011 ◽

Vol 71 (1) ◽

pp. 72-82 ◽

Cited By ~ 94

Author(s):

Xin Wang ◽

Yuan Hu ◽

Lei Song ◽

Hongyu Yang ◽

Weiyi Xing ◽

...

Keyword(s):

Flame Retardant ◽

Epoxy Resins ◽

Synthesis And Characterization

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Green synthesis and characterization of phosphorus flame retardant crosslinking agents for epoxy resins

Journal of Applied Polymer Science ◽

10.1002/app.40105 ◽

2013 ◽

Vol 131 (7) ◽

pp. n/a-n/a ◽

Cited By ~ 18

Author(s):

Andrea Toldy ◽

Beáta Szolnoki ◽

István Csontos ◽

György Marosi

Keyword(s):

Green Synthesis ◽

Flame Retardant ◽

Epoxy Resins ◽

Synthesis And Characterization ◽

Crosslinking Agents

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Synthesis and characterization of some polyimide-epoxy composites

e-Polymers ◽

10.1515/epoly.2011.11.1.244 ◽

2011 ◽

Vol 11 (1) ◽

Cited By ~ 2

Author(s):

Toheed Akhter ◽

Humaira Masood Siddiqi ◽

Zareen Akhter ◽

M. Saeed Butt

Keyword(s):

Thermal Behavior ◽

Epoxy Resins ◽

Analytical Techniques ◽

Char Yield ◽

Epoxy Composites ◽

Hydroxyl Group ◽

Synthesis And Characterization ◽

Tetracarboxylic Acid ◽

Epoxy Amine

AbstractComposites from some novel polyimide and commercial epoxy were prepared aiming to improve the thermal behavior of epoxy resins. Two diamines namely 4-4'-diamino-4''-hydroxytriphenyl methane (DHTM) and 4-4'- diaminotriphenyl methane (DTM) were synthesized by reacting aniline and aldehydes according to a reported method. The synthesized diamines were blended with commercially available epoxy 1, 4-butanedioldiglycidylether (BDDE) to synthesize model epoxy amine networks which were compared with polyimideepoxy composites. The polyimides were synthesized by reaction of these diamines with aromatic anhydride namely 3,3',4,4'-benzophenone tetracarboxylic acid dianhydride (BTDA). These synthesized polyimides were dispersed in epoxy diamine networks to prepare composites. All the monomers and composites were characterized by making use of various analytical techniques including FTIR, NMR, TGA, DSC and XRD. Presence of hydroxyl group in the diamine helped in better dispersion of polyimide leading to high Tg and high char yield at 600 °C.

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