Analysis of Trace Levels of Volatile Organic Contaminants in Municipal Drinking Water by Glass Capillary Gas Chromatography Using Simultaneous Flame Ionization and Electron Capture Detection

1980 ◽  
Vol 13 (16) ◽  
pp. 1417-1429 ◽  
Author(s):  
L. V. McCarthy ◽  
E. B. Overton ◽  
C. K. Raschke ◽  
J. L. Laseter
1985 ◽  
Vol 68 (4) ◽  
pp. 741-745
Author(s):  
Jana Chovancova ◽  
Eva Matisova ◽  
Vojtech Batora

Abstract Residues of ethylenethiourea (ETU) in grapes and wine were deter- [ mined by capillary gas chromatography and paper chromatography, without a cleanup step, and after derivatization to 5-benzyl-ETU. The ! detection limit was 0.0002 mg/kg for flame ionization detection, 0.008 mg/kg for paper chromatography with photodensitometric evaluation of the detected spot. Results were compared with a generally used GC method specifying electron capture detection of trifluoroacetylated S- benzyl-ETU. The recoveries of ETU in grapes and wine at different j concentration levels were determined. ETU residues were determined J in treated grapes but no residues were detected in wine


1979 ◽  
Vol 177 (1) ◽  
pp. 51-60 ◽  
Author(s):  
F.A. Fitzpatrick ◽  
D.A. Stringfellow ◽  
Jacques Maclouf ◽  
Michel Rigaud

Sign in / Sign up

Export Citation Format

Share Document