Experimental Comparison of Solid-state NMR Spectra for Quadrupolar Nuclei Using Various Spin-echo Sequences

2020 ◽  
Vol 49 (1) ◽  
pp. 68-70
Author(s):  
Kenjiro Hashi ◽  
Yuuki Mogami ◽  
Kenzo Deguchi ◽  
Shinobu Ohki ◽  
Atsushi Goto ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Nmr Spectra ◽  
Spin Echo ◽  
Experimental Comparison ◽  
Quadrupolar Nuclei ◽  
Spin Echo Sequences

scholarly journals Rapid acquisition of wideline MAS solid-state NMR spectra with fast MAS, proton detection, and dipolar HMQC pulse sequences

2016 ◽  
Vol 18 (36) ◽  
pp. 25284-25295 ◽  
Author(s):  
Aaron J. Rossini ◽  
Michael P. Hanrahan ◽  
Martin Thuo
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Nmr Spectra ◽  
Pulse Sequences ◽  
Quadrupolar Nuclei ◽  
Proton Detection ◽  
Rapid Acquisition ◽  
Half Integer ◽  
Fast Mas

Fast MAS and proton detection are applied to rapidly acquire wideline solid-state NMR spectra of spin-1/2 and half-integer quadrupolar nuclei.

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