Rapid Acquisition of14N Solid-State NMR Spectra with Broadband Cross Polarization

2013 ◽  
Vol 19 (48) ◽  
pp. 16469-16475 ◽  
Author(s):  
Kristopher J. Harris ◽  
Stanislav L. Veinberg ◽  
Christopher R. Mireault ◽  
Adonis Lupulescu ◽  
Lucio Frydman ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Nmr Spectra ◽  
Cross Polarization ◽  
Rapid Acquisition

scholarly journals Rapid acquisition of wideline MAS solid-state NMR spectra with fast MAS, proton detection, and dipolar HMQC pulse sequences

2016 ◽  
Vol 18 (36) ◽  
pp. 25284-25295 ◽  
Author(s):  
Aaron J. Rossini ◽  
Michael P. Hanrahan ◽  
Martin Thuo
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Nmr Spectra ◽  
Pulse Sequences ◽  
Quadrupolar Nuclei ◽  
Proton Detection ◽  
Rapid Acquisition ◽  
Half Integer ◽  
Fast Mas

Fast MAS and proton detection are applied to rapidly acquire wideline solid-state NMR spectra of spin-1/2 and half-integer quadrupolar nuclei.

Rapid Acquisition of Multidimensional Solid-State NMR Spectra of Proteins Facilitated by Covalently Bound Paramagnetic Tags

2010 ◽  
Vol 132 (28) ◽  
pp. 9561-9563 ◽  
Author(s):  
Philippe S. Nadaud ◽  
Jonathan J. Helmus ◽  
Ishita Sengupta ◽  
Christopher P. Jaroniec
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Nmr Spectra ◽  
Rapid Acquisition ◽  
Covalently Bound

Solid state NMR spectra of rapidly quenched superionic glasses composed of two lithium ortho-oxosalts

1996 ◽  
Vol 86-88 ◽  
pp. 535-538 ◽  
Author(s):  
Masanari Takahashi ◽  
Hiroshi Toyuki ◽  
Masahiro Tatsumisago ◽  
Tsutomu Minami
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Nmr Spectra

Solid State NMR Spectra of Tall Fescue Seed

1997 ◽  
pp. 255-256 ◽  
Author(s):  
J. F. Green ◽  
K. D. Gwinn ◽  
G. W. Kabalka ◽  
C. L. Anderson
Keyword(s):  
Solid State ◽  
Tall Fescue ◽  
Solid State Nmr ◽  
Nmr Spectra

Thermosetting Mechanism Study of Organosilicon Polymer Containing Carborane by Solid-State NMR Spectroscopy

1999 ◽  
Vol 576 ◽  
Author(s):  
H. Kimura ◽  
K. Okita ◽  
M. Ichitani ◽  
M. Yonezawa ◽  
T. Sugimoto
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Nmr Spectra ◽  
Main Chain ◽  
Addition Reaction ◽  
Side Chain ◽  
Mechanism Study ◽  
Nmr Method ◽  
Organosilicon Polymer ◽  
Thermal Stable

ABSTRACTThe thermosetting mechanism of an organosilicon polymer containing carborane has been studied utilizing the 13and 29Si solid-state NMR method. The polymer having C≡C bonds in the main chain and CH═CH2, Si-H bonds, and carborane in the bulky side chain, shows a very highly thermal stability in air by curing. From 13C and 29Si NMR spectra of the polymer, it was found that the intermolecular cross-linking reactions of the polymer was due to (1) the diene reaction between Ph-C≡C and C≡C and (2) the addition reaction between side chain terminal and Ph-C≡C and between CH═CH2 and Si–H, and a very highly thermal stable structure is formed.

scholarly journals Combining solid-state NMR spectroscopy with first-principles calculations – a guide to NMR crystallography

2016 ◽  
Vol 52 (45) ◽  
pp. 7186-7204 ◽  
Author(s):  
Sharon E. Ashbrook ◽  
David McKay
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Dft Calculations ◽  
First Principles ◽  
Solid State Nmr ◽  
Nmr Spectra ◽  
First Principles Calculations ◽  
Recent Developments ◽  
Future Potential ◽  
Nmr Crystallography

DFT calculations are an important tool in assigning and interpreting NMR spectra of solids: we discuss recent developments and their future potential in the context of NMR crystallography.

95Mo solid-state NMR spectra of molybdates

1988 ◽  
Vol 148 (5) ◽  
pp. 413-416 ◽  
Author(s):  
V.M. Mastikhin ◽  
O.B. Lapina ◽  
R.I. Maximovskaya
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Nmr Spectra
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