The Rapid Preparation of 2-Aminosulfonamide-1,3,4-oxadiazoles Using Polymer-Supported Reagents and Microwave Heating.

ChemInform ◽  
2005 ◽  
Vol 36 (41) ◽  
Author(s):  
Ian R. Baxendale ◽  
Steven V. Ley ◽  
Marisa Martinelli
Keyword(s):  
Microwave Heating ◽  
Rapid Preparation ◽  
Polymer Supported

The rapid preparation of 2-aminosulfonamide-1,3,4-oxadiazoles using polymer-supported reagents and microwave heating

Tetrahedron ◽  
2005 ◽  
Vol 61 (22) ◽  
pp. 5323-5349 ◽  
Author(s):  
Ian R. Baxendale ◽  
Steven V. Ley ◽  
Marisa Martinelli
Keyword(s):  
Microwave Heating ◽  
Rapid Preparation ◽  
Polymer Supported

scholarly journals Convenient Synthesis of the Immunogenic Glycolipid BbGL1

2018 ◽  
Author(s):  
Sebastián N. Jäger ◽  
Exequiel O. J. Porta ◽  
Guillermo Labadie
Keyword(s):  
Microwave Heating ◽  
Efficient Method ◽  
Good Yield ◽  
Acyl Chloride ◽  
Rapid Preparation ◽  
Highly Efficient ◽  
Convenient Synthesis

A simple and efficient method to synthesize the immunogenic glycolipid BbGL1 is introduced. Two simple steps were required to obtain the desired product in good yield. First, a highly efficient glycosylation of cholesterol using galactosyl trichloroacetimidate as a donor was performed to produce cholesteryl--D-galactoside. Finally, an efficient palmitoylation on the C6–OH of the galactose of the synthesized saponin using sym-collidine and acyl chloride under microwave heating that produced BbGL1 in good yield. The procedure is a convenient and cheaper alternative to the reported procedures allowing a rapid preparation of multiple analogs and conjugates.

scholarly journals Convenient Synthesis of the Immunogenic Glycolipid BbGL1

2018 ◽  
Author(s):  
Sebastián N. Jäger ◽  
Exequiel O. J. Porta ◽  
Guillermo Labadie
Keyword(s):  
Microwave Heating ◽  
Efficient Method ◽  
Good Yield ◽  
Acyl Chloride ◽  
Rapid Preparation ◽  
Highly Efficient ◽  
Convenient Synthesis

A simple and efficient method to synthesize the immunogenic glycolipid BbGL1 is introduced. Two simple steps were required to obtain the desired product in good yield. First, a highly efficient glycosylation of cholesterol using galactosyl trichloroacetimidate as a donor was performed to produce cholesteryl--D-galactoside. Finally, an efficient palmitoylation on the C6–OH of the galactose of the synthesized saponin using sym-collidine and acyl chloride under microwave heating that produced BbGL1 in good yield. The procedure is a convenient and cheaper alternative to the reported procedures allowing a rapid preparation of multiple analogs and conjugates.

Rapid and Efficient Synthesis of 1,2,4-Oxadiazoles Utilizing Polymer-Supported Reagents under Microwave Heating

2005 ◽  
Vol 7 (5) ◽  
pp. 925-928 ◽  
Author(s):  
Ying Wang ◽  
Reagan L. Miller ◽  
Daryl R. Sauer ◽  
Stevan W. Djuric
Keyword(s):  
Microwave Heating ◽  
Efficient Synthesis ◽  
Polymer Supported

Rapid preparation of α-FeOOH and α-Fe2O3 nanostructures by microwave heating and their application in electrochemical sensors

2014 ◽  
Vol 49 ◽  
pp. 572-576 ◽  
Author(s):  
J.Z. Marinho ◽  
R.H.O. Montes ◽  
A.P. de Moura ◽  
E. Longo ◽  
J.A. Varela ◽  
...  
Keyword(s):  
Microwave Heating ◽  
Electrochemical Sensors ◽  
Rapid Preparation
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