Structural Assignment of Fluorocyclobutenes by 19 F NMR Spectroscopy - Comparison of Calculated 19 F NMR Shielding Constants with Experimental 19 F NMR Shifts

2018 ◽  
Vol 2018 (27-28) ◽  
pp. 3867-3874 ◽  
Author(s):  
Kateřina Kučnirová ◽  
Ondřej Šimůnek ◽  
Markéta Rybáčková ◽  
Jaroslav Kvíčala
2018 ◽  
Vol 2018 (27-28) ◽  
pp. 3875-3877
Author(s):  
Kateřina Kučnirová ◽  
Ondřej Šimůnek ◽  
Markéta Rybáčková ◽  
Jaroslav Kvíčala

2001 ◽  
Vol 56 (4-5) ◽  
pp. 342-346 ◽  
Author(s):  
Max Herberhold ◽  
Silke Gerstmann ◽  
Bernd Wrackmeyer

Abstract Bis(sulfurdiimido)tin compounds of the type R2Sn[(NSN)tBu]2 [R = Me (2a), Et (2b)] re­ act with triethylborane Et3B by rearrangement and N-ethylation to give the novel aminoborane derivatives R2Sn[N(tBu)SN(Et)BEt2]2 (5a, b), in the same way as nBu3Sn(NSN)tBu (1) reacts with Et3B to give nBu3Sn[N(tBu)SN(Et)BEt2] (4). In contrast, 2c (R = tBu) and tris(sulfurdiimido)tin compounds RSn[(NSN)tBu]3 [R = Me (3a), nBu (3d)] react with Et3B mainly by Sn- and S-ethylation, accompanied by extensive decomposition. 1H, 11B , 13C, 15N and 119Sn NMR spectroscopy served for the structural assignment in solution.


2018 ◽  
Vol 57 (50) ◽  
pp. 16375-16379 ◽  
Author(s):  
Mingzhang Wang ◽  
Manman Lu ◽  
Matthew P. Fritz ◽  
Caitlin M. Quinn ◽  
In-Ja L. Byeon ◽  
...  

1990 ◽  
Vol 16 (3) ◽  
pp. 489-495 ◽  
Author(s):  
Peter C. M. van Zijl ◽  
Laszlo Ligeti ◽  
Teresa Sinnwell ◽  
Jeffry R. Alger ◽  
A. Scott Chesnick ◽  
...  

2011 ◽  
Vol 49 (11) ◽  
pp. 740-748 ◽  
Author(s):  
Andrei V. Afonin ◽  
Dmitry V. Pavlov ◽  
Alexander I. Albanov ◽  
Ekaterina P. Levanova ◽  
Galina G. Levkovskaya

1995 ◽  
Vol 33 (11) ◽  
pp. 864-870 ◽  
Author(s):  
D. C. Blakemore ◽  
A. Gilbert ◽  
A. De Bruyn ◽  
D. De Keukeleire ◽  
E. Van der Eycken

Sign in / Sign up

Export Citation Format

Share Document