Fourier Methods with Applications

Author(s):  
Martin Brokate ◽  
Pammy Manchanda ◽  
Abul Hasan Siddiqi
Keyword(s):  
Author(s):  
D. E. Johnson

Increased specimen penetration; the principle advantage of high voltage microscopy, is accompanied by an increased need to utilize information on three dimensional specimen structure available in the form of two dimensional projections (i.e. micrographs). We are engaged in a program to develop methods which allow the maximum use of information contained in a through tilt series of micrographs to determine three dimensional speciman structure.In general, we are dealing with structures lacking in symmetry and with projections available from only a limited span of angles (±60°). For these reasons, we must make maximum use of any prior information available about the specimen. To do this in the most efficient manner, we have concentrated on iterative, real space methods rather than Fourier methods of reconstruction. The particular iterative algorithm we have developed is given in detail in ref. 3. A block diagram of the complete reconstruction system is shown in fig. 1.


1959 ◽  
Vol 27 (6) ◽  
pp. 433-434 ◽  
Author(s):  
Philip Franklin ◽  
Horace M. Trent

1. The nature of X-rays X-rays were discovered in 1895 by Rontgen in Wurtzburg. For the next 17 years the nature of these rays was one of the dominant questions in physics: were they particles or were they waves? W.H. Bragg, of Adelaide, found indisputable evidence that they were particles; C.G. Barkla, of Liverpool and Edinburgh, found even more indisputable evidence that they were waves. The decisive experiment was carried out by Friedrich and Knipping (1) in 1912 in Munich, under the guidance of von Laue; they passed a fine beam of X-rays through a crystal of copper sulphate, hoping that it would behave as a diffraction grating. It did! The background was emotionally described bv von Laue in 1948 (2). * W.H. Bragg had a son, W.L. Bragg, who was a research student under J.J. Thomson at Cambridge. He was, as he himself said later, rather upset that his father seemed to have been proved wrong, and he tried to think up an alternative explanation of particles travelling through tunnels in the crystal. But he soon realized that the wave explanation had to be accepted.


1976 ◽  
Vol 31 (3) ◽  
pp. 342-344 ◽  
Author(s):  
Volker Bätzel

Using three dimensional X-ray data collected on a four circle diffractometer, the structure of (CO)9Co3COBBr2N(C2H5)3 was solved by Patterson and Fourier methods. Least squares refinement with a block-diagonal matrix leads to a reliability index of R = 10.7%. Crystal data: α = 13.277(6) Å, b = 10.17(1) Å, c = 9.22(2) Å; α = 91.12(6)°, β = 87.61(4)°, γ = 98.79(2)°; space group P1̅; Z = 2; V = 1229,7 Å3; Dx = 1.97 gcm-3.


2016 ◽  
Vol 21 (1) ◽  
Author(s):  
Fabián Crocce ◽  
Juho Häppölä ◽  
Jonas Kiessling ◽  
Raúl Tempone

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