Determination of heavy metals in environmental reference materials using solid sampling graphite furnace AAS

1987 ◽  
Vol 328 (4-5) ◽  
pp. 405-409 ◽  
Author(s):  
G. Schlemmer ◽  
B. Welz
Keyword(s):  
Heavy Metals ◽  
Reference Materials ◽  
Graphite Furnace ◽  
Solid Sampling ◽  
Environmental Reference ◽  
Graphite Furnace Aas

scholarly journals Quality and safety of some commercial spices brands

2013 ◽  
pp. 1-9 ◽  
Author(s):  
Slavica Blagojevic ◽  
Stevan Blagojevic ◽  
Natasa Pejic ◽  
Biljana Begovic ◽  
Spasenka Gajinov
Keyword(s):  
Heavy Metals ◽  
Graphite Furnace ◽  
Microwave Digestion ◽  
Hydride Generation ◽  
Absorption Spectrometry ◽  
Human Consumption ◽  
Quality And Safety ◽  
Sweet Basil ◽  
Graphite Furnace Aas

In this study, in order to evaluate the quality and safety of selected commercial spices brands, contents of moisture and minerals, as well as the concentration of certain heavy metals (As, Hg and Pb) were determined in oregano, sweet basil, parsley and celery. The spice samples were subjected to microwave digestion, and were analyzed by atomic absorption spectrometry (AAS), using hydride generation AAS technique, cold vapor AAS technique, and graphite furnace AAS technique for determination of As, Hg and Pb, respectively. Maximum concentrations of As and Pb were determined in the same brand sample of celery, and are 0.75 ppm and 0.40 ppm, respectively, while the maximum concentration of Hg in various brands sweet basil samples is 0.05 ppm. According to the results, the contents of moisture and minerals, as well as the concentrations of heavy metals in all selected spices were below the maximum permissible limits declared by the national legislations, and are safe for human consumption.

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