Structural, morphological and electrical properties of new type Dy doped Ca6-xNa2Y2(SiO4)6(OH)2 hydroxyapatite compound synthesized by co – precipitation method

Author(s):  
Ananya Rout ◽  
Sadhana Agrawal
2015 ◽  
Vol 645-646 ◽  
pp. 1339-1344 ◽  
Author(s):  
Yan Ting Yin ◽  
Qing Hua Chen ◽  
Ting Ting Yan ◽  
Qing Hua Chen

The objective of this study was to develop a novel silica modified large-sized hydroxyapatite whiskers with improved properties for use in bone repair applications. Large-sized whiskers with a mean length of 250μm were obtained by a hydrothermal co-precipitation method at 150°C, 7.5Mpa in high-pressure reactor. Silica modified hydroxyapatite whiskers were prepared by dissolving TEOS in ethanol solution, then sintering with hydroxyapatite. The compositional and morphological properties of prepared whiskers were studied by means of x-ray diffraction (XRD), Fouier transform infrared (FT-IR), scanning electron microscopy (SEM). The results indicated the evidence of nanosilicon dioxide particles on the surface of HAP whiskers. The size of nanosilicon dioxide particles depends on dropping and stirring rate. Hence, this new type of silica modified large-sized hydroxyapatite whiskers is a valuable candidate for biomedical applications.Key words: hydroxyapatite, hydrothermal co-precipitation, surface modified, whiskers


2020 ◽  
Vol 761 ◽  
pp. 137989
Author(s):  
Tariq Munir ◽  
Naeem ur Rehman ◽  
Arslan Mahmood ◽  
Khalid Mahmood ◽  
Adnan Ali ◽  
...  

2022 ◽  
Vol 9 (1) ◽  
pp. 105-118
Author(s):  
Endi Suhendi ◽  
◽  
Andini Eka Putri ◽  
Muhamad Taufik Ulhakim ◽  
Andhy Setiawan ◽  
...  

<abstract> <p>In this study, we used a natural resource, yarosite minerals, as a Fe<sub>2</sub>O<sub>3</sub> precursor. Yarosite minerals were used for the synthesis of LaFeO<sub>3</sub>/Fe<sub>2</sub>O<sub>3</sub> doped with ZnO via a co-precipitation method using ammonium hydroxide, which produced a light brown powder. Then, an ethanol gas sensor was prepared using a screen-printing technique and characterized using gas chamber tools at 100,200, and 300 ppm of ethanol gas to investigate the sensor's performance. Several factors that substantiate electrical properties such as crystal and morphological structures were also studied using X-Ray Diffraction (XRD) and Scanning Electron Microscopy (SEM), respectively. The crystallite size decreased from about 61.4 nm to 28.8 nm after 0.5 mol% ZnO was added. The SEM characterization images informed that the modified LaFeO<sub>3</sub> was relatively the same but not uniform. Lastly, the sensor's electrical properties exhibited a high response of about 257% to 309% at an operating temperature that decreased from 205 ℃ to 180 ℃. This finding showed that these natural resources have the potential to be applied in the development of ethanol gas sensors in the future. Hence, yarosite minerals can be considered a good natural resource that can be further explored to produce an ethanol gas sensor with more sensitive response. In addition, this method reduces the cost of material purchase.</p> </abstract>


2011 ◽  
Author(s):  
Japinder Kaur ◽  
Tsering Namgyal ◽  
Sandeep Bansal ◽  
Sonal Singhal ◽  
S. K. Tripathi ◽  
...  

RSC Advances ◽  
2016 ◽  
Vol 6 (22) ◽  
pp. 17980-17986 ◽  
Author(s):  
Ali Omar Turky ◽  
Mohamed Mohamed Rashad ◽  
Ali Mostafa Hassan ◽  
Elsayed M. Elnaggar ◽  
Mikhael Bechelany

We report on the synthesis and characterization of lanthanum strontium manganite with tunable optical, magnetic and electrical properties.


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