HPHT preparation and Micro-Raman characterization of polycrystalline diamond compact with low residual stress

2010 ◽  
Vol 53 (8) ◽  
pp. 1445-1448 ◽  
Author(s):  
HongSheng Jia ◽  
HongAn Ma ◽  
Wei Guo ◽  
XiaoPeng Jia
Author(s):  
Maria C. Garcia Toro ◽  
Miguel L. Crespillo ◽  
Jose Olivares ◽  
Joseph T. Graham

2016 ◽  
Vol 2016 ◽  
pp. 1-6 ◽  
Author(s):  
A. M. Espinoza-Rivas ◽  
M. A. Pérez-Guzmán ◽  
R. Ortega-Amaya ◽  
J. Santoyo-Salazar ◽  
C. D. Gutiérrez-Lazos ◽  
...  

Graphite-coated iron nanoparticles were prepared from magnetite nanoparticles by chemical vapour deposition (CVD) under methane and hydrogen atmosphere. After being purified from carbon excess, graphite-coated iron nanoparticles were tested for morphological and magnetic properties. It was found that, during the thermal process, magnetite nanoparticles 6 nm in size coalesce and transform into graphite-coated iron 200 nm in size, as revealed by scanning electron microscopy (SEM). Raman characterization assessed that high-quality graphite coats the iron core. Magnetic measurements revealed the phase change (magnetite to iron) as an increase in the saturation magnetization from 50 to 165 emu/g after the CVD process.


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