Reduction Behavior of Surface Oxide on Submicron Copper Particles for Pressureless Sintering Under Reducing Atmosphere

Author(s):  
Tomoki Matsuda ◽  
Daiki Yamagiwa ◽  
Hideki Furusawa ◽  
Kenji Sato ◽  
Hisashi Yashiro ◽  
...  
2014 ◽  
Vol 59 (3) ◽  
pp. 947-950 ◽  
Author(s):  
A. Romański ◽  
T. Tokarski ◽  
D. Tyrała

Abstract The main objective of this paper was to perform sinterability studies of ball-milled Fe-12%Ni-6.4%Cu-1.6%Sn-0.6%C powders. A mixture of precisely weighed amounts of elemental iron, nickel and graphite, and pre-alloyed 80/20 bronze powders was ball-milled for 8, 30 and 120 hours. After cold-pressing at 400 MPa the specimens were sintered at 900oC for 30 minutes in a reducing atmosphere and subsequently tested for density and hardness as well as subjected to structural studies using scanning electron microscopy (SEM) and X-ray diffraction (XRD) analysis. The obtained results showed that only the powder ball-milled for 120 hours yielded a near pore-free material after consolidation by cold pressing and pressureless sintering at 900°C. Assuch, it could have a potential to be used in production of diamond-impregnated wire saw beads.


1997 ◽  
Vol 17 (13) ◽  
pp. 1555-1563 ◽  
Author(s):  
G. Urretavizcaya ◽  
J.M. Porto López ◽  
A.L. Cavalieri

2001 ◽  
Vol 87 (12) ◽  
pp. 756-761 ◽  
Author(s):  
Kiyotaka ITO ◽  
Masahiro KOIKE
Keyword(s):  

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