Low-temperature synthesis and characterization of the single chalcopyrite phase CuInS2 compound by vacuum sintering method

2009 ◽  
Vol 487 (1-2) ◽  
pp. L1-L4 ◽  
Author(s):  
Zhendong Wang ◽  
Xiaoliang Mo ◽  
Juan Li ◽  
Dalin Sun ◽  
Guorong Chen
Keyword(s):  
Low Temperature ◽  
Synthesis And Characterization ◽  
Vacuum Sintering ◽  
Low Temperature Synthesis ◽  
Temperature Synthesis ◽  
Sintering Method

scholarly journals Low temperature synthesis and characterization of Mn3O4 nanoparticles

2007 ◽  
Vol 5 (1) ◽  
pp. 169-176 ◽  
Author(s):  
Abdülhadi Baykal ◽  
Yüksel Köseoğlu ◽  
Mehmet Şenel
Keyword(s):  
Particle Size ◽  
Infrared Spectroscopy ◽  
Low Temperature ◽  
Synthesis And Characterization ◽  
Low Temperature Synthesis ◽  
Temperature Synthesis ◽  
X Ray ◽  
Peak Broadening ◽  
Mn3o4 Nanoparticles

AbstractHeating hydrous manganese (II) hydroxide gel at 85 °C for 12 hours produces Mn3O4 nanoparticles. They were characterized by X-ray powder diffraction (XRD) and infrared spectroscopy (FTIR). The particle size estimated from the SEM and X-ray peak broadening is approximately 32 nm, showing them to be nanocrystalline. EPR measurements confirm a typical Mn2+signal with a highly resolved hyperfine structure.

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