scholarly journals Iron, copper, zinc and bromine mapping in cirrhotic liver slices from patients with hemochromatosis studied by microscopic synchrotron radiation X-ray fluorescence analysis in continuous scanning mode

2007 ◽  
Vol 62 (6-7) ◽  
pp. 682-688 ◽  
Author(s):  
W. Osterode ◽  
G. Falkenberg ◽  
R. Höftberger ◽  
F. Wrba
1988 ◽  
Vol 42 (7) ◽  
pp. 1250-1253 ◽  
Author(s):  
C. T. Yap

The method of total reflection fluorescence analysis was used to obtain concentrations of iron, copper, zinc, and bromine in human sera. It was first applied to the commercial control-serum preparation known as Seronorm, and the results obtained were in good agreement with quoted values. The method was then used to determine the concentrations of iron, copper, zinc, and bromine in a random sampling of 62 individuals in an essentially Chinese population. The results are discussed. We feel that this is a suitable method for trace-element analysis of blood in an average laboratory. It is rapid, simple, and economical, besides being multielemental and nondestructive and requiring very small quantities—which seems to be a must in pediatrics.


2021 ◽  
Vol 11 (8) ◽  
pp. 2114-2119
Author(s):  
Chenglin Liu ◽  
Xiaohua Wang ◽  
Qiang Zhang ◽  
Dongliang Chen ◽  
Juncai Dong

Acupuncture and moxibustion are commonly accepted treatments in traditional Chinese medicine (TCM). One of the important issues of interest is determining the accurate location of acupoints in acupuncture. Modern high-technology methods were utilized to verify the accuracy of acupoint positions in TCM, reducing the uncertainty of manually locating the positions. The acupoint location was established according to the richness of trace elements (TEs). The relative content of TEs was perceived by X-ray fluorescence (XRF) analysis. The distribution of TEs was determined after the dates were calibrated and the processes were optimized. The relative content of TEs was significantly different in acupoint and non-acupoint areas. There was an uneven distribution of calcium, iron, copper, and zinc in the sample. The relative content of these elements was increased in the acupuncture areas, and the standard deviation was also relatively large, especially for calcium, showing obvious enrichment. According to the enriched area of the TEs, the distance was about 6 mm between the conception channel and the kidney meridian, and the distance to the stomach meridian was about 23 mm for the rabbit sample. The position of the acupoints and spacing of meridians, which were determined according to the enrichment of TEs, were consistent with the TCM theory. The results show that synchrotron radiation-based XRF is a suitable method for determining the location of acupoints.


Author(s):  
Cristiane Calza ◽  
Marcelino J. Anjos I ◽  
Sheila M.F. Mendonça de Souza ◽  
Antonio Brancaglion Jr ◽  
Ricardo T. Lopes

This work evaluates the chemical composition of pigments used in decorative paintings in the coffin cartonage fragments and linen wrappings of an Egyptian mummy, using X-ray microfluorescence with synchrotron radiation technique. The measures were obtained at the XRF beamline of the National Synchrotron Radiation Laboratory (LNLS). This Roman period female mummy is one of the most important mummies in the National Museum because of its unconventional embalming with disarticulated legs and arms. X-ray fluorescence analysis is a widely used spectroscopic technique in archaeometry for investigating the chemical composition of pigments in manuscripts, paintings, ceramics and other artifacts, metal alloys, and stones. Knowledge of composition allows pigment characterization through major or minor constituents, and makes it possible to establish the provenance, age, and consequently, the authenticity of the artifact.


2009 ◽  
Vol 21 (5) ◽  
pp. 927-945 ◽  
Author(s):  
Sylvia Schmitz ◽  
Andreas Möller ◽  
Max Wilke ◽  
Wolfgang Malzer ◽  
Birgit Kanngiesser ◽  
...  

2009 ◽  
Vol 54 (5) ◽  
pp. 420-423 ◽  
Author(s):  
Tsunenori Matsunaga ◽  
Hidetaka Ishizaki ◽  
Shuji Tanabe ◽  
Yoshihiko Hayashi

1992 ◽  
pp. 995-1000 ◽  
Author(s):  
J. V. Gilfrich ◽  
E. F. Skelton ◽  
S. B. Qadri ◽  
N. E. Moulton ◽  
D. J. Nagel ◽  
...  

Author(s):  
K. Janssens ◽  
F. Adams ◽  
M.L. Rivers ◽  
K.W. Jones

Micro-SXRF (Synchrotron X-ray Fluorescence) or micro-SRIXE (Synchrotron Radiation Induced X-ray Emission) is a microanalytical technique which combines the sensitivity of more conventional microchemical methods such as Secondary Ion Microscopy (SIMS) and μ-PIXE (Proton Induced X-ray Emission) with the non-destructive and quantitative character of X-ray fluorescence analysis. The detection limits attainable at current SXRF-facilities are situated in the ppm (and in favourable cases the sub-ppm) range. The sensitivity of SRIXE can be used advantageously in individual particle analysis. This type of analysis is used, e.g., for studying sources of athmospheric pollution. Analysis of standard NIST micro-spheres at the NSLS-SRIXE facility yielded minimum detection limits in the 1 to 100 ppm range for particle sizes of around 10 to 30 μm.An interesting approach to individual particle characterisation is by means of electron microprobe analysis (EPMA). By using the backscattered electron signals, in an automated fashion, particles can be easily located on a filter substrate and their size and shape determined.


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