AbstractOne of the uncertain aspects in the analysis of x-ray spectra is the determination of the proper background to subtract from the raw data. In those cases where the background is a smoothly varying funct ion of the x-ray energy, the application of a digital filter to the raw data will effectively remove the background leaving only the filtered peak information. These filtered peaks can then be fit by using a non-linear least squares method in conjunction with a suitably chosen mathematical model of the peak structure.
A New Least-squares Method for Determination of Lattice Parameters from Powder X-ray Diffraction Data