scholarly journals NMR lipid profiles of cells, tissues, and body fluids: proton NMR analysis of human erythrocyte lipids.

1994 ◽  
Vol 35 (11) ◽  
pp. 1925-1931
Author(s):  
R K Adosraku ◽  
G T Choi ◽  
V Constantinou-Kokotos ◽  
M M Anderson ◽  
W A Gibbons
1991 ◽  
Vol 29 (6) ◽  
pp. 594-602 ◽  
Author(s):  
Mariano Casu ◽  
Graeme J. Anderson ◽  
Gregory Choi ◽  
William A. Gibbons

1978 ◽  
Vol 56 (6) ◽  
pp. 789-793 ◽  
Author(s):  
Donald C. Wigfield ◽  
Steve Feiner

The stereoisomers of 2-methyltetrahydropyran-4-ol have been separated and identified by carbon-13 and proton nmr analysis of the trideuteriomethyl-2,6,6-trideuterio analogue. Stereoisomeric product ratios of reduction of 2-methyltetrahydropyran-4-one (1) by NaBH4, KBH4, L-Selectride, K-Selectride, and LiBH(nBu)3 have been determined and compared with reductions of 3-methylcyclohexanone. Product ratios in the reduction of the two substrates by the borohydride reducing agents are similar but are quite different in the reduction by the Selectride reducing agents, 1 being reduced by Selectride to give 73% equatorialalcohol. Two possible mechanisms of reduction of 1 are proposed, involving intramolecular assistance by the cyclic ether oxygen.


2006 ◽  
Vol 12 (6) ◽  
pp. 705-710 ◽  
Author(s):  
Heide L Kirschenlohr ◽  
Julian L Griffin ◽  
Sarah C Clarke ◽  
Ranyl Rhydwen ◽  
Andrew A Grace ◽  
...  

1983 ◽  
Vol 105 (4) ◽  
pp. 733-735 ◽  
Author(s):  
Clifford J. Unkefer ◽  
Robert E. London ◽  
Thomas W. Whaley ◽  
Guido H. Daub
Keyword(s):  

Synlett ◽  
2017 ◽  
Vol 28 (18) ◽  
pp. 2449-2452
Author(s):  
Scott Sieburth ◽  
Yingjian Bo

A rapid and extremely simple method for silyl anion analysis is presented. The progress of silyllithium reagent preparation can be determined by quenching an aliquot with neat chloro(trimethyl)silane, evaporation, dilution with CDCl3, and direct proton NMR analysis. This procedure is fast, simple, and allows for identification and relative quantification of the starting reagent, intermediates, and the silyllithium product.


2011 ◽  
Vol 4 (1) ◽  
pp. 57-69
Author(s):  
Iago Pinal-Fernandez ◽  
Manuel Martin-Pastor ◽  
Pedro Ferro-Gallego ◽  
Lourdes Dominguez-Gerpe

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