Investigating the Dynamic Properties of the Transmembrane Segment of Phospholamban Incorporated into Phospholipid Bilayers Utilizing2H and15N Solid-State NMR Spectroscopy†

Biochemistry ◽  
2004 ◽  
Vol 43 (44) ◽  
pp. 13899-13909 ◽  
Author(s):  
Elvis K. Tiburu ◽  
Ethan S. Karp ◽  
Paresh C. Dave ◽  
Krishnan Damodaran ◽  
Gary A. Lorigan
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Dynamic Properties ◽  
Phospholipid Bilayers ◽  
Transmembrane Segment ◽  
Solid State Nmr Spectroscopy

scholarly journals Use of Solid-State NMR Spectroscopy for the Characterization of Molecular Structure and Dynamics in Solid Polymer and Hybrid Electrolytes

Polymers ◽  
2021 ◽  
Vol 13 (8) ◽  
pp. 1207
Author(s):  
Gabrielle Foran ◽  
Nina Verdier ◽  
David Lepage ◽  
Cédric Malveau ◽  
Nicolas Dupré ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Pulse Sequence ◽  
Dynamic Properties ◽  
Double Resonance ◽  
Solid Polymer ◽  
Pulse Field ◽  
Solid State Nmr Spectroscopy

Solid-state NMR spectroscopy is an established experimental technique which is used for the characterization of structural and dynamic properties of materials in their native state. Many types of solid-state NMR experiments have been used to characterize both lithium-based and sodium-based solid polymer and polymer–ceramic hybrid electrolyte materials. This review describes several solid-state NMR experiments that are commonly employed in the analysis of these systems: pulse field gradient NMR, electrophoretic NMR, variable temperature T1 relaxation, T2 relaxation and linewidth analysis, exchange spectroscopy, cross polarization, Rotational Echo Double Resonance, and isotope enrichment. In this review, each technique is introduced with a short description of the pulse sequence, and examples of experiments that have been performed in real solid-state polymer and/or hybrid electrolyte systems are provided. The results and conclusions of these experiments are discussed to inform readers of the strengths and weaknesses of each technique when applied to polymer and hybrid electrolyte systems. It is anticipated that this review may be used to aid in the selection of solid-state NMR experiments for the analysis of these systems.

scholarly journals Side Chain and Backbone Dynamics of Phospholamban in Phospholipid Bilayers Utilizing2H and15N Solid-State NMR Spectroscopy†

Biochemistry ◽  
2007 ◽  
Vol 46 (42) ◽  
pp. 11695-11706 ◽  
Author(s):  
Shadi Abu-Baker ◽  
Jun-Xia Lu ◽  
Shidong Chu ◽  
Clarke C. Brinn ◽  
Christopher A. Makaroff ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Phospholipid Bilayers ◽  
Backbone Dynamics ◽  
Side Chain ◽  
Solid State Nmr Spectroscopy

Fibrillation mechanism of glucagon in the presence of phospholipid bilayers as revealed by 13C solid-state NMR spectroscopy

2019 ◽  
Vol 219 ◽  
pp. 36-44 ◽  
Author(s):  
Izumi Yamane ◽  
Ayano Momose ◽  
Hideki Fujita ◽  
Eri Yoshimoto ◽  
Akie Kikuchi-Kinoshita ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Phospholipid Bilayers ◽  
Solid State Nmr Spectroscopy

scholarly journals Orientation of Cecropin A Helices in Phospholipid Bilayers Determined by Solid-State NMR Spectroscopy

1999 ◽  
Vol 77 (6) ◽  
pp. 3152-3155 ◽  
Author(s):  
Francesca M. Marassi ◽  
Stanley J. Opella ◽  
Padmaja Juvvadi ◽  
R.B. Merrifield
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Phospholipid Bilayers ◽  
Solid State Nmr Spectroscopy ◽  
Cecropin A
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