Effects of hydrothermal synthesis conditions on high purity TiO2 preparation via sulfate process

Author(s):  
Congxue Tian
2013 ◽  
Vol 807-809 ◽  
pp. 591-595
Author(s):  
Hong Liang Chen ◽  
Ji Song Yang ◽  
Yan Wang ◽  
Hui Ying Li ◽  
Xin Xin Li ◽  
...  

High performance silicalite-1 membranes were successfully synthesized on silica tubes by seeding method after filling the tubes with water and glycerol mixtures. After seeding the silica tubes with 200 nm seeds, all the silicalite-1 membranes show acceptable separation performance towards ethanol/water mixture after 4-12 h hydrothermal synthesis, and the highest flux of membrane with 8 h hydrothermal synthesis reaches about 0.98 kg/m2.h and the separation factor reaches about 60 towards 3 wt.% ethanol/water mixture. This result shows that the as-synthesized silicalite-1 membrane can concentrate the ethanol from 3% to about 65%, and the ethanol can be obtained over 600 g/m2.h by using the silicalite-1 membrane, which shows that seeding method and suitable control of synthesis conditions is possible for preparing high-performance silicalite-1 membranes.


CrystEngComm ◽  
2014 ◽  
Vol 16 (24) ◽  
pp. 5418-5423 ◽  
Author(s):  
Yan Chen ◽  
Mingyu Shang ◽  
Xiaofeng Wu ◽  
Shouhua Feng

In this work, a green chemistry strategy was developed to synthesize blue pigments SrCuSi4O10 and BaCuSi4O10 with good yield and high purity. SrCuSi4O10 and BaCuSi4O10 exhibit hierarchical structures. Our study shows that hydrothermally synthesized BaCuSi2O6 exhibits interesting broad near-infrared luminescence.


2021 ◽  
Vol 47 (2) ◽  
pp. 2809-2821 ◽  
Author(s):  
Evgeniya A. Syukkalova ◽  
Anastasia V. Sadetskaya ◽  
Natalya D. Demidova ◽  
Natalia P. Bobrysheva ◽  
Mikhail G. Osmolowsky ◽  
...  

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