scholarly journals In situ exsolution of Ni particles on the PrBaMn2O5 SOFC electrode material monitored by high temperature neutron powder diffraction under hydrogen

2020 ◽  
Vol 8 (7) ◽  
pp. 3590-3597 ◽  
Author(s):  
Mona Bahout ◽  
Praveen B. Managutti ◽  
Vincent Dorcet ◽  
Annie Le Gal La Salle ◽  
Serge Paofai ◽  
...  
Keyword(s):  
High Temperature ◽  
Anode Material ◽  
Powder Diffraction ◽  
Electrode Material ◽  
Hydrogen Atmosphere ◽  
Neutron Powder Diffraction ◽  
Ni Catalyst

NiO has been incorporated into the Pr0.5Ba0.5MnO3−δ perovskite to produce in situ exsolved Ni-catalyst on the PrBaMn2O5 anode material upon heating under a hydrogen atmosphere.

scholarly journals The High-Temperature Transformation from 1T- to 3R-LixTiS2 (x = 0.7, 0.9) as Observed in situ with Neutron Powder Diffraction

2015 ◽  
Vol 229 (9) ◽  
Author(s):  
Dennis Wiedemann ◽  
Suliman Nakhal ◽  
Anatoliy Senyshyn ◽  
Thomas Bredow ◽  
Martin Lerch
Keyword(s):  
High Temperature ◽  
Powder Diffraction ◽  
Electrode Material ◽  
Room Temperature ◽  
Lithium Ion ◽  
Neutron Powder Diffraction ◽  
Titanium Disulfide ◽  
Temperature Transformation

AbstractLayered titanium disulfide is used as lithium-ion intercalating electrode material in batteries. The room-temperature stable trigonal 1T polymorphs of the intercalates Li

Mn-Mg disordering in cummingtonite: a high-temperature neutron powder diffraction study

2000 ◽  
Vol 64 (2) ◽  
pp. 255-266 ◽  
Author(s):  
J. J. Reece ◽  
S. A. T. Redfern ◽  
M. D. Welch ◽  
C. M. B. Henderson
Keyword(s):  
Crystal Structure ◽  
Phase Transition ◽  
New York ◽  
High Temperature ◽  
Powder Diffraction ◽  
Elevated Temperatures ◽  
Neutron Powder Diffraction ◽  
Site Preference ◽  
A Site

AbstractThe crystal structure of a manganoan cummingtonite, composition [M4](Na0.13Ca0.41Mg0.46Mn1.00) [M1,2,3](Mg4.87Mn0.13)(Si8O22)(OH)2, (Z = 2), a = 9.5539(2) Å, b = 18.0293(3) Å, c = 5.2999(1) Å, β = 102.614(2)° from Talcville, New York, has been refined at high temperature using in situ neutron powder diffraction. The P21/m to C2/m phase transition, observed as spontaneous strains +ε1 = −ε2, occurs at ˜107°C. Long-range disordering between Mg2+ and Mn2+ on the M(4) and M(2) sites occurs above 550°C. Mn2+ occupies the M(4) and M(2) sites preferring M(4) with a site-preference energy of 24.6±1.5 kJ mol−1. Disordering induces an increase in XMnM2 and decrease in XMnM4 at elevated temperatures. Upon cooling, the ordered states of cation occupancy are ‘frozen in’ and strains in lattice parameters are maintained, suggesting that re-equilibration during cooling has not taken place.

In situ high-temperature X-ray and neutron powder diffraction study of cation partitioning in synthetic Mg(Fe0.5Al0.5)2O4 spinel

2010 ◽  
Vol 38 (1) ◽  
pp. 11-19 ◽  
Author(s):  
Nicoletta Marinoni ◽  
Davide Levy ◽  
Monica Dapiaggi ◽  
Alessandro Pavese ◽  
Ronald I. Smith
Keyword(s):  
High Temperature ◽  
Diffraction Study ◽  
Powder Diffraction ◽  
Neutron Powder Diffraction ◽  
X Ray

scholarly journals Stability of NdBaCo2−xMnxO5+δ (x = 0, 0.5) layered perovskites under humid conditions investigated by high-temperature in situ neutron powder diffraction

2015 ◽  
Vol 3 (30) ◽  
pp. 15420-15431 ◽  
Author(s):  
Mona Bahout ◽  
Stevin S. Pramana ◽  
James M. Hanlon ◽  
Vincent Dorcet ◽  
Ronald I. Smith ◽  
...  
Keyword(s):  
High Temperature ◽  
Powder Diffraction ◽  
Neutron Powder Diffraction ◽  
Layered Perovskites

NdBaCo2O5+δ Rietveld fit at 600 °C in wet air and SAED at RT along [11̄0] after 40 h of heating in a wet atmosphere.

In situ high temperature neutron powder diffraction study of oxygen-rich La2NiO4+δin air: correlation with the electrical behaviour

2006 ◽  
Vol 16 (33) ◽  
pp. 3402-3408 ◽  
Author(s):  
A. Aguadero ◽  
J. A. Alonso ◽  
M. J. Martínez-Lope ◽  
M. T. Fernández-Díaz ◽  
M. J. Escudero ◽  
...  
Keyword(s):  
High Temperature ◽  
Diffraction Study ◽  
Powder Diffraction ◽  
Neutron Powder Diffraction ◽  
Electrical Behaviour
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