Nucleation-tuned Mechanism to Prepare Centre-crossed Zeolite Lamellas by Rotating/static Switch Crystallization Strategy

Author(s):  
Jing Wang ◽  
Xinlan Zhang ◽  
Lihua Chen ◽  
Xinhuan Lu ◽  
Qinghua Xia ◽  
...  

Although it is normally considered that hydrothermal synthesis is difficult to be controlled, the controllable synthesis of zeolite and related materials is believed to be possible by tuning the crystal...

RSC Advances ◽  
2015 ◽  
Vol 5 (96) ◽  
pp. 78457-78467 ◽  
Author(s):  
Lei Zhang ◽  
Jin-Song Hu ◽  
Cheng-Ling Pan ◽  
Xin-Hua Huang ◽  
Chang-Min Hou

Novel Bi25VO40 microcubes were successfully prepared via a facile hydrothermal synthesis route and they exhibited excellent optical and catalytic properties.


2013 ◽  
Vol 634-638 ◽  
pp. 2203-2206
Author(s):  
Geng Zhu ◽  
Feng Tao ◽  
Cong Rong Hu ◽  
Zhi Jun Wang ◽  
Hai Tao Zhang ◽  
...  

EuF3nanorods with 400 nm in average diameter and 950 nm in length have been synthesized via a hydrothermal method at low temperature. The phase and shape of the products were characterized by XRD, SEM, HRTEM and SAED. Studies show that the chelating agent EDTA is vital to the morphology of the final product. Under longer UV excitation, the as-prepared EuF3nanorods emitted the yellow and red light. This method will find its applications in exploring the crystal growth process and provide guidance for the morphology controllable synthesis.


RSC Advances ◽  
2016 ◽  
Vol 6 (9) ◽  
pp. 7448-7454 ◽  
Author(s):  
Niraj Kumar ◽  
P. Dineshkumar ◽  
R. Rameshbabu ◽  
Arijit Sen

A simple one-pot hydrothermal synthesis of single crystalline β-MnO2 nanorods with diameters in the range of 10–40 nm is reported.


2019 ◽  
Vol 14 (5) ◽  
pp. 493-495 ◽  
Author(s):  
Qinghua Yang ◽  
Chunni Xiao ◽  
Bingbing Chen ◽  
Lin Ma ◽  
Limei Xu

2020 ◽  
Author(s):  
Xiaojing Xia ◽  
Anupum Pant ◽  
Xuezhe Zhou ◽  
Elena Dobretsova ◽  
Alex Bard ◽  
...  

Fluoride crystals, due to their low phonon energies, are attractive hosts of trivalent lanthanide ions for applications in upconverting phosphors, quantum information science, and solid-state laser refrigeration. In this article, we report the rapid, low-cost hydrothermal synthesis of potassium lutetium fluoride (KLF) microcrystals for applications in solid-state laser refrigeration. Four crystalline phases were synthesized, namely orthorhombic K<sub>2</sub>LuF<sub>5</sub> (Pnma), trigonal KLuF<sub>4</sub> (P3<sub>1</sub>21), orthorhombic KLu<sub>2</sub>F<sub>7</sub> (Pna2<sub>1</sub>), and cubic KLu<sub>3</sub>F<sub>10</sub> (Fm3m), with each phase exhibiting unique microcrystalline morphologies. Luminescence spectra and emission lifetimes of the four crystalline phases were characterized based on the point-group symmetry of trivalent cations. Laser refrigeration was measured by observing both the optomechanical eigenfrequencies of microcrystals on cantilevers in vacuum, and also the Brownian dynamics of optically trapped microcrystals in water. Among all four crystalline phases, the most significant cooling was observed for 10%Yb:KLuF<sub>4</sub> with cooling of 8.6 $\pm$ 2.1 K below room temperature. Reduced heating was observed with 10%Yb:K<sub>2</sub>LuF<sub>5</sub>


2013 ◽  
Vol 28 (3) ◽  
pp. 287-294 ◽  
Author(s):  
Guo-Cong LIU ◽  
Zhen JING ◽  
Xi-Bing ZHANG ◽  
Xian-Feng LI ◽  
Hong LIU

2009 ◽  
Vol 24 (6) ◽  
pp. 1110-1114 ◽  
Author(s):  
Ji-Yuan ZHANG ◽  
Han-Min TIAN ◽  
Zhi-Peng TIAN ◽  
Xiang-Yan WANG ◽  
Tao YU ◽  
...  

Sign in / Sign up

Export Citation Format

Share Document