Measurement and calculation of resolution of time-of-flight small-angle neutron scattering

1986 ◽  
Vol 19 (5) ◽  
pp. 311-319 ◽  
Author(s):  
D. F. R. Mildner ◽  
J. M. Carpenter ◽  
D. L. Worcester
2017 ◽  
Vol 45 (5) ◽  
pp. 541-557 ◽  
Author(s):  
Rong Du ◽  
Haolai Tian ◽  
Taisen Zuo ◽  
Ming Tang ◽  
Lili Yan ◽  
...  

2007 ◽  
Vol 40 (1) ◽  
pp. 40-50 ◽  
Author(s):  
B. Grabcev

Analytic forms are found for resolution functions of small-angle neutron scattering instruments. The expressions are developed as a function of momentum transfer (Q) rather than separately in terms of neutron wavelength (λ) and scattering angle (θ). Effects caused by the gravitational field as well as by quasi-elastic scattering are included. Explicit analytic forms for the transmission functions are proposed for both the incident and scattered beams, enabling careful analysis of any problem regarding small-angle scattering experiments. Due to the reciprocal mathematical relationship between λ, θ andQ, [λ, θ] space is employed to approach different aspects of the topic. Applications to time-of-flight instruments with rectangular apertures, including the choice of the most convenient instrumental parameters, the analysis of smearing effects and the data reduction toQspace, are presented.


2003 ◽  
Vol 36 (3) ◽  
pp. 763-768 ◽  
Author(s):  
J.M. Carpenter ◽  
M. Agamalian ◽  
K.C. Littrell ◽  
P. Thiyagarajan ◽  
Ch. Rehm

2015 ◽  
Vol 48 (6) ◽  
pp. 1849-1859 ◽  
Author(s):  
Aurel Radulescu ◽  
Noémi Kinga Székely ◽  
Stephan Polachowski ◽  
Marko Leyendecker ◽  
Matthias Amann ◽  
...  

Following demand from the user community regarding the possibility of improving the experimental resolution, the dedicated high-intensity/extendedQ-range SANS diffractometer KWS-2 of the Jülich Centre for Neutron Science at the Heinz Maier-Leibnitz Center in Garching was equipped with a double-disc chopper with a variable opening slit window and time-of-flight (TOF) data acquisition option. The chopper used in concert with a dedicated high-intensity velocity selector enables the tuning at will of the wavelength resolution Δλ/λ within a broad range, from 20% (standard) down to 2%, in a convenient and safe manner following pre-planned or spontaneous decisions during the experiment. The new working mode is described in detail, and its efficiency is demonstrated on several standard samples with known properties and on a completely new crystallizable copolymer system, which were investigated using both the conventional (static) and TOF modes.


2019 ◽  
Vol 52 (1) ◽  
pp. 1-12 ◽  
Author(s):  
Anna Sokolova ◽  
Andrew E. Whitten ◽  
Liliana de Campo ◽  
Jason Christoforidis ◽  
Andrew Eltobaji ◽  
...  

BILBY is a recently constructed and commissioned time-of-flight small-angle neutron scattering instrument, operated by the Australian Centre for Neutron Scattering at the Australian Nuclear Science and Technology Organisation (ANSTO). BILBY provides a wide accessible q range (q ≃ 1.0 × 10−3 Å−1 to ∼1.8 Å−1) and variable wavelength resolution (Δλ/λ ≃ 3–30%) to complement the other small-angle and ultra-small-angle neutron scattering capabilities available at ANSTO. Since its construction, BILBY has been used to study samples from a wide range of scientific disciplines, including biology, chemistry, physics and materials science. This article describes the BILBY design and components, and shows data collected from a number of reference samples.


2009 ◽  
Vol 167 (1) ◽  
pp. 73-79 ◽  
Author(s):  
W. Kreuzpaintner ◽  
J.-F. Moulin ◽  
D. Lott ◽  
R. Kampmann ◽  
M. Haese-Seiller ◽  
...  

2014 ◽  
Vol 47 (4) ◽  
pp. 1228-1237 ◽  
Author(s):  
Peter Müller-Buschbaum ◽  
Gunar Kaune ◽  
Martin Haese-Seiller ◽  
Jean-Francois Moulin

The complex nanomorphology of a defect-rich deuterated poly(styrene-block-methyl methacrylate), P(S-b-MMAd), diblock copolymer film is determined with a combination of grazing-incidence small-angle neutron scattering (GISANS) and time-of-flight (TOF) mode. TOF-GISANS enables the simultaneous performance of several GISANS measurements that differ in wavelength. The resulting set of GISANS data covers different ranges of the scattering vector and has different scattering depths. Thus surface-sensitive and bulk-sensitive measurements can be performed simultaneously. The P(S-b-MMAd) film exhibits a lamellar microphase separation structure, which because of the defects is arranged into small, randomly oriented grains, composed of four–five lamellar repetitions. In the near-surface region, the lamellar structure is oriented parallel to the substrate, which explains the smooth surface found with atomic force microscopy.


Sign in / Sign up

Export Citation Format

Share Document