Crystal structure of 2,2′-({[2-(tritylsulfanyl)benzyl]azanediyl}bis(ethane-2,1-diyl))bis(isoindoline-1,3-dione)
2014 ◽
Vol 70
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pp. o895-o896
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In the structure of the title compound, C46H37N3O4S, the planes of the two isoindoline units make a dihedral angle of 77.86 (3)°. The dihedral angles between the benzyl plane and the isoindoline units are 79.56 (4) and 3.74 (9)°. The geometry at the S atom shows a short [1.7748 (17) Å] S—Cbenzyland a long [1.8820 (15) Å] S—Ctritylbond and the C—S—C angle is 108.40 (7)°. N—C bond lengths around the azane N atom are in the range 1.454 (2)–1.463 (2) Å. he crystal packing exhibts two rather `non-classical' C—H...O hydrogen bonds that result in stacking of the molecules along theaas well as thebaxis and give rise to columnar sub-structures.
2014 ◽
Vol 70
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pp. o1122-o1123
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2012 ◽
Vol 68
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pp. o1857-o1857
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2006 ◽
Vol 62
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pp. o1419-o1420
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2020 ◽
Vol 76
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pp. 1209-1212
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2006 ◽
Vol 62
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pp. o1279-o1280
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2014 ◽
Vol 70
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pp. o917-o918
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2012 ◽
Vol 68
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pp. o2556-o2557
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2012 ◽
Vol 68
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pp. o1023-o1023
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2013 ◽
Vol 69
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pp. o1719-o1720
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2018 ◽
Vol 74
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pp. 1746-1750
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