Determination of nanoobject sizes and concentrations in irradiated metals and alloys via positron annihilation spectroscopy

Author(s):  
V. I. Grafutin ◽  
E. P. Prokop’ev ◽  
V. Krsjak ◽  
R. Burcl ◽  
P. Häehner ◽  
...  
2008 ◽  
Vol 278 ◽  
pp. 15-24
Author(s):  
M. Abdel-Rahman ◽  
Yahia A. Lotfy ◽  
M.A. Abdel-Rahman ◽  
Emad A. Badawi

Positron Annihilation Spectroscopy (PAS) is a powerful and versatile tool for the study of the microscopic structure of materials. Doppler Broadening Positron Annihilation Technique (DBPAT) is the fastest technique used among positron annihilation techniques. The dose effect in Al-6.5at. % Cu alloy was investigated by means of DBPAT. An abrupt change in both the S and W line-shape parameter values occurred at 70 kGy of irradiation. The S- and W-Parameters of the trapped positrons at 70 kGy of γ−irradiation dose are about 48 % and 14 % respectively. The S- versus W-parameter reveals a linear relationship indicating the presence of only one type of defect. The S- and W-parameters have been used in the determination of the positron trapping rate and the grain size of the AlCu6.5 alloy.


1984 ◽  
Vol 41 ◽  
Author(s):  
R. W. Siegel ◽  
M. J. Fluss ◽  
L. C. Smedskjaer

AbstractPositrons localize in trapped states at a variety of defect sites in solids, from which they subsequently annihilate with unique observable characteristics. As such, the positron is a valuable probe for the study of these defects. Positron annihilation spectroscopy (PAS) has made significant contributions in recent years to the determination of atomic defect properties in metals and alloys, and in molecular solids as well. It has also been used extensively in the monitoring and characterization of vacancy-like microstructure development, as occurs during post-irradiation annealing. The characterization of defects using PAS is selectively reviewed and some possibilities for using the positron as a localized probe of the atomic and electronic structure of atomic defects and their aggregates are discussed.


2011 ◽  
Vol 40 (6) ◽  
pp. 428-435 ◽  
Author(s):  
V. I. Grafutin ◽  
I. N. Meshkov ◽  
E. P. Prokop’ev ◽  
N. O. Khmelevskii ◽  
S. L. Yakovenko

2009 ◽  
Vol 58 (12) ◽  
pp. 8478
Author(s):  
Wang Qiao-Zhan ◽  
Yu Run-Sheng ◽  
Qin Xiu-Bo ◽  
Li Yu-Xiao ◽  
Wang Bao-Yi ◽  
...  

2014 ◽  
Vol 12 (12) ◽  
pp. 1280-1284
Author(s):  
Konstantin Arefyev ◽  
Victor Grafutin ◽  
Evgeny Prokopyev ◽  
Andrey Lider ◽  
Roman Laptev ◽  
...  

AbstractThis article considers the possibility of applying the positron annihilation spectroscopy method for investigating the pore space of rocks from oil-gas and methane-coal deposits. The diagnostics of the structure was performed using the method of spectrometry of angular correlation of annihilation rays (ACAR). Using the samples of porous silicon, the authors have shown the applicability of the ACAR method for determination of the average dimensions of spherical and cylindrical nanosized objects and their concentration


2007 ◽  
Vol 75 (20) ◽  
Author(s):  
A. Zubiaga ◽  
J. A. García ◽  
F. Plazaola ◽  
F. Tuomisto ◽  
J. Zúñiga-Pérez ◽  
...  

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