scholarly journals Method Validation for the Determination of Phthalates in Indoor Air by GC-MS with Solid-Phase Adsorption/Solvent Extraction using Octadecyl Silica Filter and Styrene–Divinylbenzene Copolymer Cartridge

BPB Reports ◽  
2019 ◽  
Vol 2 (5) ◽  
pp. 86-90
Author(s):  
Toshiko Tanaka-Kagawa ◽  
Ikue Saito ◽  
Aya Onuki ◽  
Maiko Tahara ◽  
Tsuyoshi Kawakami ◽  
...  
Keyword(s):  
Solvent Extraction ◽  
Method Validation ◽  
Indoor Air ◽  
Solid Phase ◽  
Octadecyl Silica ◽  
Styrene Divinylbenzene ◽  
Solid Phase Adsorption

scholarly journals Multiresidue Determination of Organophosphorus Pesticides in Ginkgo Leaves by Accelerated Solvent Extraction and Gas Chromatography with Flame Photometric Detection

2005 ◽  
Vol 88 (3) ◽  
pp. 729-735
Author(s):  
Xionghai Yi ◽  
Yitong Lu
Keyword(s):  
Gas Chromatography ◽  
Solvent Extraction ◽  
Solid Phase ◽  
Organophosphorus Pesticides ◽  
Accelerated Solvent Extraction ◽  
Simple Method ◽  
Photometric Detection ◽  
Relative Standard ◽  
Flame Photometric Detection

Abstract A rapid and simple method using accelerated solvent extraction and solid-phase extraction cleanup was developed and validated for the determination of 15 organophosphorus pesticides in ginkgo leaves by capillary gas chromatography with flame photometric detection. The pesticides were extracted at 100°C under 1500 psi pressure in <20 min. The average recovery from 10 g ginkgo leaves, fortified at 3 levels ranging from 0.05 to 1.00 mg/kg, was 95.2% with a relative standard deviation of 4.6%. The limits of detection ranged from 1.11 × 10−3 mg/kg (dimethoate) to 4.44 × 10−3 mg/kg (dichlorvos). The proposed method showed acceptable accuracy and precision while minimizing environmental concerns, time, and labor. Furthermore, the method could be easily applied to the monitoring of these 15 organophosphorus pesticides in ginkgo leaves.

Development of a method based on sorbent trapping followed by solid-phase microextraction for the determination of synthetic musks in indoor air

2009 ◽  
Vol 1216 (14) ◽  
pp. 2805-2815 ◽  
Author(s):  
Jorge Regueiro ◽  
Carmen Garcia-Jares ◽  
Maria Llompart ◽  
J. Pablo Lamas ◽  
Rafael Cela
Keyword(s):  
Indoor Air ◽  
Solid Phase Microextraction ◽  
Solid Phase ◽  
Synthetic Musks
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