Application of microprecipitation on membrane filters for Alpha Spectrometry, liquid scintillation counting and Mass Spectrometric determination of plutonium isotopes

2002 ◽  
Vol 90 (9-11) ◽  
Author(s):  
E. Hrnecek ◽  
L. A. de las Heras ◽  
M. Betti

SummaryFor the determination of plutonium isotopes in environmental samples, chemical separation of plutonium together with a suitable sample preparation method for measurement is necessary. In this work, a combined method for the determination ofThe use of this approach gives the advantage of combining the strengths of both radiometric and mass spectrometric methods for plutonium determination after chemical separation from environmental samples.Results from the measurement of reference materials and from sediment samples from the Irish Sea are presented and the applied methods are compared with respect to their detection limits for the investigated nuclides.

2004 ◽  
Vol 92 (3) ◽  
Author(s):  
Jean Aupiais

SummaryThe reliability and accuracy of actinide measurement in environmental samples strongly depend on theThe intensity of the internal conversions for thorium, uranium, plutonium and americium have been calculated and normalised to the intensity of the main alpha transition. These data can be used to determine the activity of any above-mentioned actinide by alpha liquid scintillation with alpha/beta discrimination. The quantitative analysis and the isotopic ratio determination of several certified solutions of actinides demonstrate the validity of this approach.


2017 ◽  
Vol 995 ◽  
pp. 1-20 ◽  
Author(s):  
Wenting Bu ◽  
Jian Zheng ◽  
Michael E. Ketterer ◽  
Sheng Hu ◽  
Shigeo Uchida ◽  
...  

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