Use of generalised pole figures in the X-ray study of textured metal materials

2007 ◽  
Vol 2007 (suppl_26) ◽  
pp. 327-332
Author(s):  
Yu. Perlovich ◽  
M. Isaenkova ◽  
V. Fesenko
Keyword(s):  
X Ray ◽  
2004 ◽  
Vol 443-444 ◽  
pp. 259-262 ◽  
Author(s):  
Yuriy Perlovich ◽  
Margarita Isaenkova

The substructure inhomogeneity of real textured metal materials was studied by use of the X-ray method of Generalized Pole Figures and the computer data treatment. Main regularities of substructure inhomogeneity were revealed for the first time. Substructure conditions of grains in rolled material form an extremely wide spectrum and vary by passing from texture maxima to texture minima, where residual deformation effects are most significant. The distribution of residual elastic microstrains in the orientational space of rolled material shows the distinct system.


2010 ◽  
Vol 160 ◽  
pp. 31-38 ◽  
Author(s):  
Yuriy Perlovich ◽  
Margarita Isaenkova ◽  
Vladimir Fesenko

For systematic study of the distribution of residual deformation effects in textured metal materials the method of Generalized Pole Figures was developed, combining texture measurement with X-ray line profile measurements in such a manner that the profile of the same X-ray line (hkl) is registered by each successive position of the sample. The obtained totality of profiles after that or another treatment is used for construction of Generalized Pole Figures (GPF), i.e. distributions of measured diffraction parameters or calculated substructure parameters in the stereographic projection of the sample depending on the orientation of reflecting crystallographic planes. As applied to metal materials with developed rolling textures it was found that any volume ~1 mm3 is characterized by an extremely wide spectrum of substructure conditions. Three laws of substructure anisotropy were revealed for the first time. The 1st law: Residual deformation effects are minimal along directions, corresponding to maximal density of crystallographic axes, i.e. texture maxima, and increase up to highest values by passing to texture minima. The 2nd law concerns variation of lattice parameters in metal products due to elastic microstrain: For each grain with crystalline lattice, extended along axis <hkl> by (+ε), there is its pair with the symmetric orientation, where along axis <hkl> crystalline lattice is compressed by (-ε), so that accompanying elastic microstresses are equilibrated. The 3rd law: By passing from residual tension of the crystalline lattice to its compression, grain fragmentation changes depending on indexes of the reference axis, i.e. tensile and compressive elastic deformations of the crystalline lattice differ in their uniformity.


2005 ◽  
Vol 495-497 ◽  
pp. 77-86
Author(s):  
Yuriy Perlovich ◽  
Margarita Isaenkova ◽  
Vladimir Fesenko ◽  
Hans Joachim Bunge

The substructure nonuniformity of metal materials with developed deformation texture was studied by use of the X-ray method of Generalized Pole Figures. Main regularities of substructure nonuniformity were revealed for the first time. Substructure conditions of grains in rolled material form an extremely wide spectrum and vary by passing from texture maxima to texture minima, where residual deformation effects are most significant. The distribution of residual elastic microstrains in the orientational space of rolled material shows the distinct cross-wise system, consisting in alternation of quadrants with predominant microstrains of opposite signs.


2007 ◽  
Vol 2007 (suppl_26) ◽  
pp. 327-332 ◽  
Author(s):  
Yu. Perlovich ◽  
M. Isaenkova ◽  
V. Fesenko
Keyword(s):  
X Ray ◽  

2003 ◽  
Vol 779 ◽  
Author(s):  
Yuriy Perlovich ◽  
Margarita Isaenkova ◽  
Vladimir Fesenko

AbstractThe substructure inhomogeneity of real textured metal materials was studied by use of recently developed methods of X-ray diffractometry and data treatment. Main regularities of substructure inhomogeneity were revealed for the first time by the analysis of generalized pole figures. The structure of deformed metal includes an extremely wide spectrum of substructure conditions. The crystallographic orientation of grains is the most effective criterion for systematization of substructure inhomogeneities in textured materials. The dispersity of grains and the distortion of their crystalline lattice are minimal in texture maxima and increase up to highest values by passing to texture minima. The distribution of lattice elastic deformation in rolled metals most often shows a cross-wise pattern, consisting in alternation of quadrants with predominance of elastic extension or elastic compression.


2007 ◽  
Vol 550 ◽  
pp. 253-258 ◽  
Author(s):  
Yuriy Perlovich ◽  
Margarita Isaenkova ◽  
Vladimir Fesenko

The substructure inhomogeneity of real textured metal materials was studied by use of the X-ray method of Generalized Pole Figures. Main regularities of substructure inhomogeneity were revealed for the first time. Substructure conditions of grains in rolled material form an extremely wide spectrum and vary by passing from texture maxima to texture minima, where residual deformation effects are most significant. The distribution of residual elastic microstrains in the orientational space of rolled material shows the distinct cross-wise system, consisting in alternation of quadrants with predominant microstrains of opposite signes.


1999 ◽  
Vol 33 (1-4) ◽  
pp. 303-319 ◽  
Author(s):  
Yu. Perlovich ◽  
H. J. Bunge ◽  
M. Isaenkova ◽  
V. Fesenko

In order to study the distribution of lattice elastic microstresses in textured metal materials, pole figures of X-ray line peak position were constructed on the basis of data, obtained by diffractometric texture measurements using a position sensitive detector. The data treatment involves recalculation of the Bragg angle 2θϕψ into the relative deviation of the interplanar spacing from the weighted average level Δd/dav. Depending on the texture character, different modes of microstress equilibrium take place. A common feature of most lattice deformation pole figures is the cross-wise pattern, consisting in alternation of quadrants with predominance of lattice elastic extension and compression. In cases of simple rolling textures, the microstress equilibrium is attained by some additional ways, among which there are breaking of texture maxima into halves with opposite signs of elastic deformation, predominance of one-sign elastic deformation within different texture maxima, development of stretched zones with opposite signs of elastic deformation at slopes of texture maxima. In some cases the identical microstress distribution in all quadrants of pole figure is observed.


2005 ◽  
Vol 495-497 ◽  
pp. 827-832 ◽  
Author(s):  
Margarita Isaenkova ◽  
Yuriy Perlovich ◽  
Vladimir Fesenko ◽  
M. Grekhov ◽  
Igor V. Alexandrov ◽  
...  

Texture analysis and the new X-ray method of Generalized Pole Figures (GPF) were used by the study of texture and substructure inhomogeneity of Ti rods, submitted to Equal-Channel Angular Pressing (ECAP) at 400oC. Local texture features testify about gradual rotation of loading axes by ~15o when crossing the rod’s section. As a result of second pass (route C), the specific ECAP texture weakens and the textureless component intensifies. Observed substructure changes are connected with development of dynamic recovery and dynamic recrystallization.


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