scholarly journals Study on Ultraminiature Thermal Analysis Device with Micro-Air-Bridge Heater and a New Method for its Heating-rate Curve

1999 ◽  
Vol 119 (3) ◽  
pp. 119-124 ◽  
Author(s):  
Jun-ichi Hayasaka ◽  
Chikako Sawai ◽  
Mitsuteru Kimura

2012 ◽  
Vol 110 (1) ◽  
pp. 17-25 ◽  
Author(s):  
Toshihiro Fujii
Keyword(s):  


2019 ◽  
Vol 16 (31) ◽  
pp. 235-241
Author(s):  
Mariana Fornazier BORGES

The present work seeks to demonstrate through a series of experiments such as the parameters heating rate, type of stand and physical form of the sample, can influence the qualitative and quantitative aspects of the results of the thermal analyzes of TGA and DSC. To do this, polyvinyl alcohol, a synthetic polymer was used as a model and its thermal behavior was discussed by the results obtained by the thermogravimetric (TGA) and DSC curves, showing the effect of the alteration of each parameter, such as the displacement at the temperature at which the thermal events occur in the TGA curves, related to the alteration of the physical form of the sample; the intensification of the DSC peaks due to the increase of the heating rate, the change in the heat flow by changing the stand and masking some events such as the glass transition temperature.



1988 ◽  
Vol 13 (3) ◽  
pp. 319-336
Author(s):  
J. M. Dorkel ◽  
A. Napieralski ◽  
Ph. Leturcq


2009 ◽  
Vol 66 ◽  
pp. 77-80 ◽  
Author(s):  
Ge Sun ◽  
Hao Wang ◽  
Wei Min Wang ◽  
Yu Cheng Wang ◽  
Zheng Yi Fu

Ultra-fine zirconium diboride (ZrB2) powders have been synthesized by borothermal reduction reaction, using zirconium oxychloride (ZrOCl2•8H2O) as the precursors of zirconia. The thermodynamic variation in the amorphous ZrO2-B system was studied by thermogravimetric and differential thermal analysis (TG-DTA). The precursors containing amorphous ZrO2 and B were heat-treated under a high heating rate. It is shown that the borothermal reaction can be completed at a relatively low temperature (~950 °C) and short duration (~5 min) under a heating rate of 200 °C/min. The synthesized powders have an average crystalline size of 300 nm with oxygen content less than 2.62 wt%.



1976 ◽  
Vol 14 (1-2) ◽  
pp. 169-181 ◽  
Author(s):  
A.J. Beardell ◽  
J. Staley ◽  
C. Campbell


1980 ◽  
Vol PAS-99 (6) ◽  
pp. 2386-2392 ◽  
Author(s):  
M. M. Aziz ◽  
H. Riege
Keyword(s):  


2017 ◽  
Vol 3 (2) ◽  
pp. 43-51 ◽  
Author(s):  
Ana X. H. Yong ◽  
Graham D. Sims ◽  
Samuel J. P. Gnaniah ◽  
Stephen L. Ogin ◽  
Paul A. Smith


2015 ◽  
Vol 1095 ◽  
pp. 468-470
Author(s):  
Ling Liu ◽  
Zheng Xing ◽  
Yi Xiang Liu ◽  
Hua Yi

The main influence factors on thermal analysis of medium-density fiberboard (MDF) was analyzed by thermo-gravimetry (TG) and derivative thermo-gravimetry (DTG) , which are heating rate, atmosphere and sample . Results showed that heating rate affected the thermo-decomposition obviously, while the effect on the residual charcoal was small, The results can provide reference to extinguishment and fire investigation.



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