Surface-steps formed during the cleavage of MgO on {100} planes, the smaller steps of which may be of atomic height, have been observed in Reflection-Electron Microscopy investigations to be accurately aligned along <001> directions. Steps of atomic height also have been identified on MgO smoke-particle platelets; these steps may be curved or straight, with the straight steps showing evidence for faceting along <001>. Reference also is made to faceting along <011> and <012> directions. Straight steps ∼2 unit cells high, with edges along <100> also have been imaged by High-Resolution Profile-Imaging at the peripheries of MgO smoke microcubes. After etching in aqua-regia and annealing in air, however, high densities of “large” steps several unit cells high, as well as numerous holes, are formed. It is faceting in these foils that is reported here.As can be seen in fig 1, obvious faceting of the surface-step traces is extremely rare in these foils, in marked contrast to substrates such as LaAlO3 and SrTiO3, on which surface-step traces facet readily after a similar preparation treatment.
A Fundamental Study of Platinum Recovery from Spent Auto-Catalyst Using “Dry Aqua Regia”
