Neutron Strain Scanning of Archaeological Bronzes

2006 ◽  
Vol 524-525 ◽  
pp. 975-980 ◽  
Author(s):  
Javier R. Santisteban ◽  
S. Siano ◽  
Mark R. Daymond

We report neutron strain scanning experiments on archaeological bronzes, with the aim of identifying the original manufacturing techniques used. The specimens studied were a Picenan necklace from VI BC, and an Etruscan bucket handle from IV BC, exhibited at the Marches Museum of Archaeology, Ancona, Italy. Time-of-flight neutron diffraction and transmission experiments were performed at the ENGIN-X instrument, ISIS, UK. For the necklace, characteristic bending strain profiles and a small degree of preferred orientation indicate that the specimen had been cold worked. For the handle, broad diffraction peaks and highly distorted Bragg edges -typical of a columnar grain microstructure- suggested that this specimen was cast and did not undergo significant thermal or mechanical treatment. The relation between the experimental diffracted and transmitted time-of-flight spectra, and the microstructure of specimens are discussed.

2021 ◽  
Vol 5 (2) ◽  
pp. 12
Author(s):  
Matthew M. Schmitt ◽  
Daniel J. Savage ◽  
James J. Wall ◽  
John D. Yeager ◽  
Chanho Lee ◽  
...  

The US code of Federal Regulations mandates regular inspection of centrifugally cast austenitic stainless steel pipe, commonly used in primary cooling loops in light-water nuclear power plants. These pipes typically have a wall thickness of ~8 cm. Unfortunately, inspection using conventional ultrasonic techniques is not reliable as the microstructure strongly attenuates ultrasonic waves. Work is ongoing to simulate the behavior of acoustic waves in this microstructure and ultimately develop an acoustic inspection method for reactor inspections. In order to account for elastic anisotropy in the material, the texture in the steel was measured as a function of radial distance though the pipe wall. Experiments were conducted on two 10 × 12.7 × 80 mm radial sections of a cast pipe using neutron diffraction scans of 2 mm slices using the HIPPO time-of-flight neutron diffractometer at the Los Alamos Neutron Science Center (LANSCE, Los Alamos, NM, USA). Strong textures dominated by a small number of austenite grains with their (100) direction aligned in the radial direction of the pipe were observed. ODF analysis indicated that up to 70% of the probed volume was occupied by just three single-grain orientations, consistent with grain sizes of almost 1 cm. Texture and phase fraction of both ferrite and austenite phases were measured along the length of the samples. These results will inform the development of a more robust diagnostic tool for regular inspection of this material.


2017 ◽  
Vol 27 (4) ◽  
pp. 1-5
Author(s):  
Tsutomu Hemmi ◽  
Stefanus Harjo ◽  
Hideki Kajitani ◽  
Tomone Suwa ◽  
Toru Saito ◽  
...  

1974 ◽  
Vol 52 (8) ◽  
pp. 748-752 ◽  
Author(s):  
V. Novotny ◽  
T. M. Holden ◽  
G. Dolling

Neutron diffraction experiments on small particles of lead in the pores of Vycor glass are described. The small particles have a coherence length of (107 ± 20) Å; there is only a slight increase in the lattice parameter as compared with bulk lead, but an analysis of the intensity of the diffraction peaks reveals that there is an increase in the average amplitude of vibration of 28%. At least 80% of the lead in the glass is present in the crystalline state and contributes to the coherent diffraction.


2017 ◽  
Vol 59 (3) ◽  
pp. 607-612 ◽  
Author(s):  
A. S. Kurlov ◽  
A. I. Gusev ◽  
V. S. Kuznetsov ◽  
I. A. Bobrikov ◽  
A. M. Balagurov ◽  
...  

2006 ◽  
Vol 89 (23) ◽  
pp. 233515
Author(s):  
E. Üstündag ◽  
R. A. Karnesky ◽  
M. R. Daymond ◽  
I. C. Noyan

2006 ◽  
Vol 385-386 ◽  
pp. 1203-1205 ◽  
Author(s):  
Matthias Gutmann ◽  
Winfried Kockelmann ◽  
Laurent Chapon ◽  
Paolo G. Radaelli

2017 ◽  
Vol 7 (1) ◽  
Author(s):  
Alberto Cereser ◽  
Markus Strobl ◽  
Stephen A. Hall ◽  
Axel Steuwer ◽  
Ryoji Kiyanagi ◽  
...  

2014 ◽  
Vol 25 (2) ◽  
pp. 025602 ◽  
Author(s):  
H Suzuki ◽  
K Kusunoki ◽  
Y Hatanaka ◽  
T Mukai ◽  
A Tasai ◽  
...  

1990 ◽  
pp. 403-407 ◽  
Author(s):  
A. C. Lawson ◽  
J. W. Conant ◽  
C. L. Talcott ◽  
M. A. David ◽  
J. Vaninetti ◽  
...  

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