Although the spectrum originating from a superconducting bending magnet is quasi-continuous, it shows important intensity variations through its spectral range. A method to determine the incident energy-dependent flux variation based on the comparison between observed intensities and the calculated intensities of a well known structure (calcite) is presented here. It is found that the measured flux is highly sensitive to the use of correct Debye–Waller factors for the atoms of the standard crystal. By using the measured flux curve, it was possible to unambiguously index the Laue diffraction pattern of a trigonal crystal structure in its hexagonal setting. This is a crucial but difficult first step for the determination of strain and stress in materials with this symmetry, such as quartz, Mg, Ti, Znetc.
X-ray Laue diffraction from crystals of xylose isomerase.
