ChemInform Abstract: Preparation of Undoped Lead Titanate Ceramics via Sol-Gel Processing.

ChemInform ◽  
2010 ◽  
Vol 30 (19) ◽  
pp. no-no
Author(s):  
Sunuk Kim ◽  
Myong-cheol Jun ◽  
Soon-cheol Hwang
Keyword(s):  
Lead Titanate ◽  
Sol Gel ◽  
Titanate Ceramics ◽  
Gel Processing

scholarly journals Sol-gel processing and physic-chemical characterization of La and Ce doped lead titanate ceramics

2013 ◽  
Vol 5 ◽  
pp. 04036
Author(s):  
Y. Guaaybess ◽  
M. Maanan ◽  
R. Adhiri ◽  
M. Moussetad ◽  
A. El Mesbahi ◽  
...  
Keyword(s):  
Lead Titanate ◽  
Sol Gel ◽  
Chemical Characterization ◽  
Titanate Ceramics ◽  
Gel Processing

Preparation of Undoped Lead Titanate Ceramics via Sol-Gel Processing

2004 ◽  
Vol 82 (2) ◽  
pp. 289-296 ◽  
Author(s):  
Sunuk Kim ◽  
Myong-cheol Jun ◽  
Soon-cheol Hwang
Keyword(s):  
Lead Titanate ◽  
Sol Gel ◽  
Titanate Ceramics ◽  
Gel Processing

High-Speed Synthesis and Electric Properties of Magnesium Doped Lead Titanate Ceramics

2007 ◽  
Vol 121-123 ◽  
pp. 149-152
Author(s):  
Liang Sheng Qiang ◽  
Dong Yan Tang ◽  
Xing Hong Zhang ◽  
L. Jin
Keyword(s):  
Lead Titanate ◽  
High Speed ◽  
Sintering Temperature ◽  
Water Solution ◽  
Sol Gel ◽  
Electric Properties ◽  
Synthesis Process ◽  
Pure Lead ◽  
Alcohol Water ◽  
Titanate Ceramics

By adding methyl alcohol/water solution with certain concentration into sol to hydrolysis directly and sintering the fresh sol directly, lead titanate(PbTiO3) ceramics doped with magnesium are prepared by using magnesium acetate as doper to prohibit the disadvantages contained in conventional sol-gel method, such as low hydrolytic rate, high sintering temperature, long preparation period. The changes of structure, microstructure, synthesis process and electric properties of modified ceramics are studied in detail. The sizes and morphology of high purely and high density magnesium doped lead titanate nanocrystals thus obtained are observed by TEM photographs and the structures and affection of sintering temperature of to lattice constant and sizes of nanocrystals are detected by XRD. Electric properties detection results show that doped lead titanate ceramics exhibite excellent dielectric, ferroelectric and pyroelectric properties compare with pure lead titanate.

Synthesis of lanthanum-doped lead titanate ceramics using a modified sol–gel route and their structural analysis

2021 ◽  
Vol 585 (1) ◽  
pp. 88-96
Author(s):  
Avanish Kumar ◽  
Anju Dixit ◽  
Swati Chopra ◽  
P. S. Dobal
Keyword(s):  
Structural Analysis ◽  
Lead Titanate ◽  
Sol Gel ◽  
Titanate Ceramics

Sol-Gel Processing and Structure Development of Lead Titanate Particles

1994 ◽  
Vol 346 ◽  
Author(s):  
John S. Wright ◽  
Lorraine Falter Francis
Keyword(s):  
Lead Titanate ◽  
Isopropyl Alcohol ◽  
Perovskite Phase ◽  
Sol Gel ◽  
Amorphous Structure ◽  
Spherical Particles ◽  
Internal Surfaces ◽  
Reflectance Ftir ◽  
Gel Processing ◽  
Gel Network

ABSTRACTSpherical particles of lead titanate, PbTiO3, (PT) were prepared from partially hydrolyzed alkoxide solutions modified with benzoic acid. Modified and aged alkoxide solutions were added dropwise to isopropyl alcohol, forming particles (0.2 to 1.0 μm in diameter). FTIR spectroscopy results demonstrate chelation of the PT alkoxide which prevented the formation of an extended gel network. Diffuse reflectance FTIR (DRIFT) spectra indicate the benzoate ligands are present until 450°C; TGA results show significant weight loss at 450°C. PT particles crystallize into the perovskite phase at =450°C, as determined by DTA and XRD. The relatively low crystallization temperature may be due to the effect of benzoate ligands on amorphous structure and presence of internal surfaces.

Ferroelectric thin films of calcium modified lead titanate by sol-gel processing

1994 ◽  
Vol 13 (24) ◽  
pp. 1804-1805 ◽  
Author(s):  
R. Sirera ◽  
M. L. Calzada ◽  
F. Carmona ◽  
B. Jim�nez
Keyword(s):  
Thin Films ◽  
Lead Titanate ◽  
Sol Gel ◽  
Ferroelectric Thin Films ◽  
Gel Processing

Sol-Gel Processing of Lead Titanate in 2-Methoxyethanol: Investigations into the Nature of the Prehydrolyzed Solutions

1988 ◽  
Vol 71 (5) ◽  
pp. C-280-C-282 ◽  
Author(s):  
Thomas W. Dekleva ◽  
James M. Hayes ◽  
Leslie E. Cross ◽  
Gregory L. Geoffroy
Keyword(s):  
Lead Titanate ◽  
Sol Gel ◽  
Gel Processing

Nmr Spectroscopic Investigations of Pbtio3 Sol-Gel Processing

1990 ◽  
Vol 180 ◽  
Author(s):  
S.D. Ramamurthi ◽  
D.A. Payne
Keyword(s):  
Lead Titanate ◽  
Lead Acetate ◽  
Sol Gel ◽  
Titanium Isopropoxide ◽  
Alkoxy Group ◽  
Mass Spectrometric ◽  
Titanium Complex ◽  
Spectroscopic Investigations ◽  
Gel Processing ◽  
Mass Spectrometric Techniques

ABSTRACTLead titanate gels were prepared by sol-gel processing from lead acetate and titanium isopropoxide in methoxyethanol. In the present study, 1H, and 13C FTNMR spectroscopic and mass spectrometric techniques were used to identify the structures of lead and titanium precursors formed by refluxing lead acetate and titanium isopropoxide in methoxyethanol, respectively. Lead acetate was found to be partially alkoxylated, whereas, the titanium precursor was identified as a dimer with complete alkoxy group exchange. Similar procedures were applied to identify the lead titanium complex formed from lead and titanium precursors.

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