High-Speed Synthesis and Electric Properties of Magnesium Doped Lead Titanate Ceramics

2007 ◽  
Vol 121-123 ◽  
pp. 149-152
Author(s):  
Liang Sheng Qiang ◽  
Dong Yan Tang ◽  
Xing Hong Zhang ◽  
L. Jin
Keyword(s):  
Lead Titanate ◽  
High Speed ◽  
Sintering Temperature ◽  
Water Solution ◽  
Sol Gel ◽  
Electric Properties ◽  
Synthesis Process ◽  
Pure Lead ◽  
Alcohol Water ◽  
Titanate Ceramics

By adding methyl alcohol/water solution with certain concentration into sol to hydrolysis directly and sintering the fresh sol directly, lead titanate(PbTiO3) ceramics doped with magnesium are prepared by using magnesium acetate as doper to prohibit the disadvantages contained in conventional sol-gel method, such as low hydrolytic rate, high sintering temperature, long preparation period. The changes of structure, microstructure, synthesis process and electric properties of modified ceramics are studied in detail. The sizes and morphology of high purely and high density magnesium doped lead titanate nanocrystals thus obtained are observed by TEM photographs and the structures and affection of sintering temperature of to lattice constant and sizes of nanocrystals are detected by XRD. Electric properties detection results show that doped lead titanate ceramics exhibite excellent dielectric, ferroelectric and pyroelectric properties compare with pure lead titanate.

ChemInform Abstract: Preparation of Undoped Lead Titanate Ceramics via Sol-Gel Processing.

ChemInform ◽  
2010 ◽  
Vol 30 (19) ◽  
pp. no-no
Author(s):  
Sunuk Kim ◽  
Myong-cheol Jun ◽  
Soon-cheol Hwang
Keyword(s):  
Lead Titanate ◽  
Sol Gel ◽  
Titanate Ceramics ◽  
Gel Processing

Structural and Morphological Analysis of Solid State Synthesized Pure Lead Titanate and Calcium Doped Lead Titanate Ceramics for Ferroelectric and Piezoelectric Energy Storage Applications

2020 ◽  
Vol 837 ◽  
pp. 153-158
Author(s):  
Shubham Sharma ◽  
Xiao Nan Dong ◽  
Peng Wei ◽  
Chen Long
Keyword(s):  
Solid State ◽  
Lead Titanate ◽  
Morphological Analysis ◽  
Microstructural Analysis ◽  
Research Work ◽  
Phase Identification ◽  
Pure Lead ◽  
Piezoelectric Energy ◽  
Titanate Ceramics ◽  
Structural Characterizations

This novel research work addresses the physical properties of Lead titanate (PT), PbTiO3 sample with additives. The modification of this sample was carried out by adding calcium in proportion of 5 to 15mol%. The samples in bulk form were synthesized by utilizing traditional method of solid state synthesis. The properties like structural analysis, and grain size determination were studied for the PbTiO3 sample & for the calcium modified lead titanate (PCT). The phase identification, structural characterizations and microstructural analysis hasanalyzed in this manuscript.

Fabrication and Ferroelectric Properties of Ba-Doped Strontium Bismuth Titanate Ceramics

2007 ◽  
Vol 280-283 ◽  
pp. 163-166
Author(s):  
Dan Xie ◽  
Wei Pan ◽  
Zhi Min Dang ◽  
Tian Ling Ren
Keyword(s):  
Electron Microscopy ◽  
Remanent Polarization ◽  
Bismuth Titanate ◽  
Sintering Temperature ◽  
Ferroelectric Properties ◽  
Sol Gel ◽  
Molar Ratio ◽  
Sol Gel Process ◽  
Titanate Ceramics ◽  
Coercive Electric Field

In the paper, the microstructure and properties of Sr1-xBaxBi4Ti4O15 (SBBT) ceramics with different Ba contents were investigated. SBBT ceramics were fabricated by means of the method combining Sol-Gel process and ordinary firing. The morphology will change when Ba2+ is doped in SrBi4Ti4O15 (SBTi), which will lead to the change of structure and ferroelectric properties. The microstructure of SBTi and BaBi4Ti4O15 (BBTi) ceramics were characterized by scan electron microscopy (SEM). With the increase of Ba2+ doping contents, the sintering temperature of SBBT ceramics decreases, 1120°C for SBTi and 1060°C for BBTi. BBTi ceramics contain more and larger plate-like grains than that in SBTi, the diameter of the grains in BBTi is about 8~10 µm, the thickness is about 2.5 µm. With the increase of Ba2+ doping contents, remanent polarization (Pr) and coercive electric-field (Ec) increase first and then decrease. At the molar ratio of Sr:Ba=0.5:0.5, SBBT ceramics exhibited the highest Pr and Ec.

Synthesis of lanthanum-doped lead titanate ceramics using a modified sol–gel route and their structural analysis

2021 ◽  
Vol 585 (1) ◽  
pp. 88-96
Author(s):  
Avanish Kumar ◽  
Anju Dixit ◽  
Swati Chopra ◽  
P. S. Dobal
Keyword(s):  
Structural Analysis ◽  
Lead Titanate ◽  
Sol Gel ◽  
Titanate Ceramics

scholarly journals Sol-gel processing and physic-chemical characterization of La and Ce doped lead titanate ceramics

2013 ◽  
Vol 5 ◽  
pp. 04036
Author(s):  
Y. Guaaybess ◽  
M. Maanan ◽  
R. Adhiri ◽  
M. Moussetad ◽  
A. El Mesbahi ◽  
...  
Keyword(s):  
Lead Titanate ◽  
Sol Gel ◽  
Chemical Characterization ◽  
Titanate Ceramics ◽  
Gel Processing

Effect of TiO2 Nanopowders on the Sintering and Electric Properties of Lead Zirconate Titanate Ceramics

2007 ◽  
Vol 336-338 ◽  
pp. 228-230
Author(s):  
Guang Hui Li ◽  
Zhang Lian Hong ◽  
Li Xia Peng ◽  
Min Quan Wang
Keyword(s):  
Dielectric Properties ◽  
Bulk Density ◽  
Lead Zirconate Titanate ◽  
Sintering Temperature ◽  
Lead Zirconate ◽  
Electric Properties ◽  
Pzt Ceramics ◽  
Zirconate Titanate ◽  
Titanate Ceramics ◽  
Tio2 Nanopowder

XRD, SEM, bulk density and dielectric properties measurements were used to investigate the effect of TiO2 nanopowder substitution for conventional TiO2 micro-powder on the sintering and electric properties of PZT ceramics. Results revealed that the sintering temperature of dense Pb(Zr0.53Ti0.47)O3 ceramics was lowered about 50°C ~ 100°C when 20% and 40% of conventional TiO2 micro-powder was substituted by TiO2 nanopowder. The electric properties were kept or even enhanced in the PZT ceramics adopted the TiO2 nanopowder.

Piezoelectric properties of sol-gel-derived samarium-dysprosium-modified lead titanate ceramics

1988 ◽  
Vol 23 (6) ◽  
pp. 2087-2092 ◽  
Author(s):  
J. M. Hayes ◽  
T. R. Gururaja ◽  
L. E. Cross ◽  
G. L. Geoffroy
Keyword(s):  
Lead Titanate ◽  
Piezoelectric Properties ◽  
Sol Gel ◽  
Titanate Ceramics
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