Synthesis of some pyrazole-3-carboxylic acid-hydrazide and pyrazolopyridazine compounds

2005 ◽  
Vol 42 (1) ◽  
pp. 117-120 ◽  
Author(s):  
İ Özer İlhan ◽  
Emin Saripinar ◽  
Yunus Akçamur
2003 ◽  
Vol 68 (10) ◽  
pp. 723-727 ◽  
Author(s):  
Vijay Dabholkar ◽  
Rahul Gavande

A series of 1-(3,4-dihydro-3-oxo-2H-1,4-benzoxazine-2-carbonyl)-3-methyl-4-(substituted phenylhydrazono)-2-pyrazolin-5-ones have been synthesized by the reaction of 2H-3,4-dihydro-3-oxo-1,4-benzoxazine-2-carboxylic acid hydrazide with substituted acetoacetic ester derivatives using acetic acid as solvent under microwave irradiation (MWI), as well as by conventional methods. The reaction rate is enhanced tremendously and the yields are improved under MWI as compared to conventional methods.


2018 ◽  
Vol 54 (3) ◽  
pp. 509-511 ◽  
Author(s):  
D. S. Kopchuk ◽  
A. P. Krinochkin ◽  
E. S. Starnovskaya ◽  
Ya. K. Shtaitz ◽  
I. S. Kovalev ◽  
...  

The Analyst ◽  
2014 ◽  
Vol 139 (11) ◽  
pp. 2764-2773 ◽  
Author(s):  
Zhongxin Zhu ◽  
Xuan Zhou ◽  
Yang Wang ◽  
Lisha Chi ◽  
Dandan Ruan ◽  
...  

A sensitive, specific, economic and MS compatible staining method for gel-separated glycoproteins by using BH was described and demonstrated by 1-D and 2-D SDS-PAGE, deglycosylation, glycoprotein affinity enrichment and LC-MS/MS, respectively.


1994 ◽  
Vol 42 (2) ◽  
pp. 371-372 ◽  
Author(s):  
Muneo MORISHITA ◽  
Jun KOBAYASHI ◽  
Hiroshi YAMADA ◽  
Takehiko YAJIMA

1982 ◽  
Vol 89 (2) ◽  
pp. 235-242 ◽  
Author(s):  
C. H. Collins ◽  
M. D. Yates ◽  
J. M. Grange

SUMMARYVirulent strains of Mycobacterium tuberculosis isolated from humans are divisible into five variants by using four tests: oxygen requirement (aerobic or microaerophilic), nitrate reductase activity, susceptibility to pyrazinamide (60 μg/ml) and susceptibility to thiophene-2-carboxylic acid hydrazide (5 μg/ml). The five variants are referred to as Classical human, Asian human, bovine, African I and African II. The relation of these variants to previously described types is discussed. This simple division has been shown to be useful in epidemiological studies.


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