Multiple melting behavior of poly(butylene succinate). II. Thermal analysis of isothermal crystallization and melting process

2005 ◽  
Vol 43 (15) ◽  
pp. 2039-2047 ◽  
Author(s):  
Munehisa Yasuniwa ◽  
Shinsuke Tsubakihara ◽  
Tadashi Satou ◽  
Koji Iura

2005 ◽  
Vol 43 (21) ◽  
pp. 3077-3082 ◽  
Author(s):  
Yaming Wang ◽  
Mrinal Bhattacharya ◽  
João F. Mano


2007 ◽  
Vol 43 (8) ◽  
pp. 3163-3170 ◽  
Author(s):  
Xiaohong Wang ◽  
Jianjun Zhou ◽  
Lin Li


Polymer ◽  
2000 ◽  
Vol 41 (25) ◽  
pp. 8879-8886 ◽  
Author(s):  
S Sohn ◽  
A Alizadeh ◽  
H Marand


2013 ◽  
Vol 773 ◽  
pp. 530-533
Author(s):  
Chen Liu ◽  
Xiang Hui Lu ◽  
Xue Qi ◽  
Peng Li

The melting and recrystallization behavior of Poly(ethylene terephthalate) (PET)/ Attapulgite(At)nanocomposites after isothermal crystallization from the melt was studied by Step-scan differential scanning calorimetry (SDSC). The influence of At contents, crystallization temperature and crystallization time on the melting process were examined. Two melting endotherms(in the SDSC CP.A curves, reversible part) and one recrystallization exotherm (in the SDSC CP.IsoK curves, irreversible part)of PET/At nanocomposites after isothermal crystallization were observed during the melt process. This ascribes to the melting-recrystallization mechanism .The low temperature endotherm attributes to the melting of primary crystal formed during the isothermal treating and the high temperature endotherm resulting from the melting of recrystallization materials. The reason why more recrystallization happened with the increase of At content was given and the process of recrystallization was described in detail. The effects of crystal perfection and recrystallization were minimized by increasing of crystallization temperature and time.





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