Analysis of k0 neutron activation analysis at the University of Missouri Research Reactor

2009 ◽  
Vol 67 (6) ◽  
pp. 1084-1088 ◽  
Author(s):  
J.D. Brockman ◽  
J.D. Robertson
2012 ◽  
Vol 76 (5) ◽  
pp. 1229-1245 ◽  
Author(s):  
O. D. Osborne ◽  
A. Pring ◽  
R. S. Popelka-Filcoff ◽  
J. W. Bennett ◽  
A. Stopic ◽  
...  

AbstractThirty pyrite samples from a wide range of localities were analysed using relative comparator and k0 neutron activation analysis (NAA) techniques at the University of Missouri Research Reactor, Columbia, Missouri, USA (MURR) and the Australian Nuclear Science and Technology Organisation, Lucas Heights, NSW, Australia (ANSTO), respectively. Statistical analyses of the trace-element data produced by the two methods showed a generally good correlation, with the majority of elemental concentrations of paired data reported by MURR and ANSTO being indistinguishable at a 0.05 significance level. Trace-element analyses of pyrite from Navajún in Spain by both techniques compare well with published data. There is evidence for contamination by Al, Na and Ti in one set of samples, this is likely to have been introduced by contact with a plastic used in sample preparation.


2015 ◽  
Vol 5 (4) ◽  
pp. 23-29
Author(s):  
Thi Sy Nguyen ◽  
Manh Dung Ho ◽  
Van Doanh Ho ◽  
Quang Thien Tran ◽  
Sam Chung Yong

The k0-based neutron activation analysis (k0-NAA) has been applied for determination of trace multi-element in 5 fruits: Orange, tomato, persimmon, pear and apple. The samples were collected in Vietnam and Korea, and dried-frozen in laboratory at a temperature of -650C, weighed approximately 50 mg or 100 mg each sample, and put in clean polyethylene bags for short and long time irradiations, respectively. The NIST-1547 (Peach Leaves) and IAEA-V-10 (Hay Powder) were used for the purpose of quality control. Both analytical and standard samples were irradiated in the 500 kW Dalat research reactor (Vietnam) and the 20 MW HANARO research reactor (Korea). Concentration of 16 elements: Al, As, Au, Br, Ca, Cl, Co, Eu, Fe, K, La, Mg, Mn, Na, Rb and Zn were determined. By comparison the concentrations of trace elements in the investigated Vietnam and Korea’s fruits, revealed that they are mostly similar between two places. However, the Ca concentration in orange from Vietnam was approximately 2.5 times higher than that one from Korea, whereas the Ca concentration in pear from Vietnam was approximately 21 times lower than that one from Korea. The Mn concentrations in all of fruits that collected in Vietnam were mostly higher than those collected in Korea, ranging between 1.4 to 2.2 times.


2014 ◽  
Vol 4 (1) ◽  
pp. 84-90
Author(s):  
V. Doanh H. ◽  
D. Vu C. ◽  
Q. Thien T. ◽  
N. Son P. ◽  
T. Sy N. ◽  
...  

An auto-pneumatic transfer system has been installed at the Dalat research reactor for rapid instrument neutron activation analysis based on very short-lived nuclides. This system can be used to perform short irradiations in seconds either in the vertical channel 13-2 or in the horizontal thermal column of the reactor. The transferring time of sample from irradiation to measurement position is approximately 3.2 seconds. A loss-free counting system using HPGE detector has been also setup in compacting with the pneumatic transfer system for measurement of sample’s activity, automatically starting for data acquisition at irradiated sample’s arrival. This new facility was tested and shown to have high potential for the determination of short-lived nuclides with half-lives from 10 ¸ 100 seconds. This work presents the results of timing parameter measurements, characterization of irradiation facilities, and application of this system to determining Selenium concentration in several biological reference materials.


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