Application of response surface methodology for roasting optimization in composite roasting—Acid leaching vanadium extraction process

Author(s):  
Xin Wang ◽  
Junyi Xiang ◽  
Guishang Pei ◽  
Lanjie Li ◽  
Qingyun Huang ◽  
...  
2013 ◽  
Vol 763 ◽  
pp. 246-249
Author(s):  
Xiao Song ◽  
Peng Zhao

Flavonoids from Tussilago farfara L. was extracted with the assistance of microwave.Box-Behnken design (BBD) was employed to optimize extraction time; microwave power and ratio of water to raw material to obtain a high flavonoids yield.The optimum extraction conditions were as follows: 73.3% ethanol-water solvent, time 16.25 min and ratio of solvent to raw material 36.2ml/g.The yield of flavonoids was 11.37% based on the above mentioned conditions.


2014 ◽  
Vol 1014 ◽  
pp. 61-64
Author(s):  
Xiao Song ◽  
Peng Zhao ◽  
Qing Hua Meng ◽  
Zhi Shu Tang ◽  
Chang Li Wang

Flavonoids from Platycarya Strobi lacea Sieb.et Zucc. was extracted with the assistance of microwave.Box-Behnken design (BBD) was employed to optimize extraction time; microwave power and ratio of solvent to raw material to obtain a high flavonoids yield. The optimum extraction conditions were as follows: 65.32% ethanol-water solvent, time 3.96 min and ratio of solvent to raw material 20.8 ml/g.The yield of flavonoids was 3.41% based on the above mentioned conditions.


2018 ◽  
Vol 7 (3) ◽  
pp. 110
Author(s):  
I Gede Arie Mahendra Putra ◽  
I Wayan Rai Widarta ◽  
Putu Timur Ina

This study was aimed to determine the optimum temperature and extraction time of citrus lemon peel (Citrus limon (Linn.) Burm.F.) oleoresins by using Response Surface Methodology (RSM). The results showed that the optimum temperature and time of extraction with ultrasonic waves to produced oleoresins were 59,28ºC and 72,57 minutes. The extraction process with optimum temperature and time produced citrus lemon peel oleoresin with yield and refractive index respectively 32,47% and 1,4923. Meanwhile, the value of the density is equal to 1,3740 g/cm3 and the chemical compound was identified by GC-MS instrument. The component that was found in the citrus lemon peel oleoresin were 1-propanone, 1,3,6 Octratriene, Propanoic Acid, 2-Furancarboxaldehyde, 4-Vinyl-2-Methoxy-Phenol, 1-Pentene, Neryl Acetate, Geranic Acetate, ?-Bergamotene, Limonene, 2-Hexenal, 2-Bornanone, 2-Decyn-1-ol, Methyl Eugenol, Cis-P-Mentha-1(7),8-dien-2-ol, 1,4 Naphthalendione, Undecanal, Octadecanoic Acid, Pentadecanoic Acid, Decanoic Acid, 11-Octadecanoic Acid,GeranylButirate, Geranyl Propionate and 1,2-Benzenedicarboxylic Acid.


2019 ◽  
Vol 48 (4) ◽  
pp. 301-308 ◽  
Author(s):  
Sawinder Kaur ◽  
Paramjit S. Panesar ◽  
Sushma Gurumayum ◽  
Prasad Rasane ◽  
Vikas Kumar

Purpose The extraction of bioactive compounds such as pigments from natural sources, using different solvents, is a vital downstream process. The present study aims to investigate the effect of different variables, namely, extraction temperature, mass of fermented rice and time on the extraction process of orevactaene and flavanoid pigment from Epicoccum nigrum fermented broken rice. Design/methodology/approach Central composite rotatable design under response surface methodology was used for deducing optimized conditions. The pigments were extracted under conditions of extraction temperature (40-70°C), mass of fermented rice (0.5-1.5 g) and time (30-90 min), using water as the extraction media. The experimental data obtained were studied by analysis of variance. Data were fitted to a second-order polynomial equation using multiple regression analysis. Findings The optimum conditions generated by the software for aqueous extraction process, i.e. extraction temperature of 55.7°C, 0.79 g of fermented matter and extraction time of 56.6 min, resulted in a pigment yield of 52.7AU/g orevactaene and 77.2 AU/g flavanoid. Research limitations/implications The developed polynomial empirical model for the optimal recovery of the orevactaene and flavanoid pigments could be used for further studies in prediction of yield under specified variable conditions. Practical implications The response surface methodology helped in optimizng the conditions for the eco-friendly low-cost aqueous extarction process for orevactaene and flavanoid pigments, produced by Epicoccum nigrum during solid state fermentation of broken rice. This optimization can provide the basis for scaling up for industrial extraction process. Originality/value This paper focuses on optimizing the extraction conditions to get the maximum yield of orevactaene and flavanoid pigments, using water as the extracting media. No literature is available on the optimization of the extraction process of Epicoccum nigrum pigments, to the best of the authors’ knowledge.


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