Sensitivity enhancement of solid-state NMR spectra of half-integer spin quadrupolar nuclei using hyperbolic secant pulses: Applications to spin-5/2 nuclei

2006 ◽  
Vol 421 (4-6) ◽  
pp. 529-533 ◽  
Author(s):  
Renée Siegel ◽  
Thomas T. Nakashima ◽  
Roderick E. Wasylishen
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Nmr Spectra ◽  
Sensitivity Enhancement ◽  
Quadrupolar Nuclei ◽  
Integer Spin ◽  
Half Integer

scholarly journals Rapid acquisition of wideline MAS solid-state NMR spectra with fast MAS, proton detection, and dipolar HMQC pulse sequences

2016 ◽  
Vol 18 (36) ◽  
pp. 25284-25295 ◽  
Author(s):  
Aaron J. Rossini ◽  
Michael P. Hanrahan ◽  
Martin Thuo
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Nmr Spectra ◽  
Pulse Sequences ◽  
Quadrupolar Nuclei ◽  
Proton Detection ◽  
Rapid Acquisition ◽  
Half Integer ◽  
Fast Mas

Fast MAS and proton detection are applied to rapidly acquire wideline solid-state NMR spectra of spin-1/2 and half-integer quadrupolar nuclei.

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