Sensitivity enhancement of solid-state NMR spectra of half-integer spin quadrupolar nuclei: Double- or single-frequency sweeps? Insights from the hyperbolic secant experiment

2008 ◽  
Vol 450 (4-6) ◽  
pp. 417-421 ◽  
Author(s):  
Thomas T. Nakashima ◽  
Roderick E. Wasylishen ◽  
Renée Siegel ◽  
Kristopher J. Ooms
2016 ◽  
Vol 18 (36) ◽  
pp. 25284-25295 ◽  
Author(s):  
Aaron J. Rossini ◽  
Michael P. Hanrahan ◽  
Martin Thuo

Fast MAS and proton detection are applied to rapidly acquire wideline solid-state NMR spectra of spin-1/2 and half-integer quadrupolar nuclei.


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