Synthesis mechanism and sintering behavior of tungsten carbide powder produced by a novel solid state reaction of W2N

2012 ◽  
Vol 35 ◽  
pp. 202-206 ◽  
Author(s):  
Shi-Kuan Sun ◽  
Yan-Mei Kan ◽  
De-Wei Ni ◽  
Ji Zou ◽  
Guo-Jun Zhang
Keyword(s):  
Solid State ◽  
Tungsten Carbide ◽  
Solid State Reaction ◽  
Carbide Powder ◽  
Sintering Behavior ◽  
Synthesis Mechanism ◽  
Tungsten Carbide Powder

Sintering behavior and ionic conductivity of Li1.5Al0.5Ti1.5(PO4)3 synthesized with different precursors

2021 ◽  
Vol 0 (0) ◽  
Author(s):  
Bambar Davaasuren ◽  
Qianli Ma ◽  
Alexandra von der Heiden ◽  
Frank Tietz
Keyword(s):  
Grain Size ◽  
Solid State ◽  
Ionic Conductivity ◽  
Solid State Reaction ◽  
Sintering Temperature ◽  
Sintering Behavior ◽  
Homogeneous Microstructure ◽  
Micro Cracks ◽  
Primary Particles ◽  
Total Ionic Conductivity

Abstract Li1.5Al0.5Ti1.5(PO4)3 (LATP) powders were prepared from different NO x -free precursors using an aqueous-based solution-assisted solid-state reaction (SA-SSR). The sintering behavior, phase formation, microstructure and ionic conductivity of the powders were explored as a function of sintering temperature. The powders showed a relatively narrow temperature windows in which shrinkage occurred. Relative densities of 95% were reached upon heating between 900 and 960 °C. Depending on the morphological features of the primary particles, either homogeneous and intact microstructures with fine grains of about <2 µm in size or a broad grain size distribution, micro-cracks and grain cleavages were obtained, indicating the instability of the microstructure. Consequently, the ceramics with a homogeneous microstructure possessed a maximum total ionic conductivity of 0.67 mS cm−1, whereas other ceramics reached only 0.58 mS cm−1 and 0.21 mS cm−1.

Surface Modification Process by Electrical Discharge Machining with Tungsten Carbide Powder Mixing in Kerosene Fluid

2019 ◽  
Vol 889 ◽  
pp. 115-122
Author(s):  
Van Tao Le ◽  
Tien Long Banh ◽  
Xuan Thai Tran ◽  
Nguyen Thi Hong Minh
Keyword(s):  
Surface Roughness ◽  
Tungsten Carbide ◽  
Electrical Discharge ◽  
Alloy Powder ◽  
Electrical Discharge Machining ◽  
Carbide Powder ◽  
Micro Hardness ◽  
Hard Materials ◽  
Tungsten Carbide Powder ◽  
Better Than

Electrical discharge machining (EDM) process is widely used to process hard materials in the industry. The process of electrical discharge is changed and called PMEDM when alloy powder is added in the oil dielectric. In the current study, the effect of tungsten carbide alloy powder added in the dielectric on the surface roughness (Ra) and the micro hardness of surface (HV) status of the workpiece SKD61 after machining is investigated. Studies show that the surface roughness and the micro hardness of surface obtained by PMEDM is generally better than that by normal EDM. The method can be applied for improving surface quality such as improving strengthening of molds and machine parts.

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