X-ray powder diffraction refinement of Cu2ZnGeTe4 structure and phase diagram of the Cu2GeTe3–ZnTe system

2005 ◽  
Vol 397 (1-2) ◽  
pp. 169-172 ◽  
Author(s):  
O.V. Parasyuk ◽  
I.D. Olekseyuk ◽  
L.V. Piskach
2018 ◽  
Vol 6 (30) ◽  
pp. 14651-14662 ◽  
Author(s):  
Laura Vitoux ◽  
Marie Guignard ◽  
Jacques Darriet ◽  
Claude Delmas

Phase diagram in the NaxMoO2system (x≤ 0.5) determined using electrochemistry andin situX-ray powder diffraction.


2002 ◽  
Vol 57 (8) ◽  
pp. 868-876 ◽  
Author(s):  
H. Oppermann ◽  
M. Zhang-Preße ◽  
P. Schmidt

The pure ternary phases on the line Yb2O3-SeO2 in thermodynamical equilibrium have been synthesized by solid state reaction and characterized using X-ray powder diffraction and IR-spectroscopy. There exist three phases: Yb2SeO5, Yb2Se3O9 and Yb2Se4O11, the last one with a homogeneiety range extending a higher SeO2-content. The thermal decompositions have been determined by total pressure measurements, and the thermodynamical data of the compounds have been derived. The phase diagram and the phase barogram have been established using the results of thermal analysis and total pressure measurements.


ChemInform ◽  
2006 ◽  
Vol 37 (26) ◽  
Author(s):  
I. D. Olekseyuk ◽  
V. P. Sachanyuk ◽  
O. V. Parasyuk

1982 ◽  
Vol 37 (3) ◽  
pp. 390-391 ◽  
Author(s):  
M. Schulte-Kellinghaus ◽  
V. Krämer

Abstract The title compounds were prepared by chemical vapour transport. They crystallize in the space group P3̅m 1 with the lattice parameters a = 7.532(3) (7.589(5)) and c = 36.54(2) (36.70(5))!. X-ray powder diffraction data are listed and the T,x phase diagram of the system AlInS3-In2S3 is shown.


ChemInform ◽  
2005 ◽  
Vol 36 (38) ◽  
Author(s):  
O. V. Parasyuk ◽  
I. D. Olekseyuk ◽  
L. V. Piskach

1997 ◽  
Vol 12 (4) ◽  
pp. 259-263 ◽  
Author(s):  
J. M. Loezos ◽  
T. A. Vanderah ◽  
J. P. Cline

X-ray powder diffraction data and refined unit cell parameters for three compounds found during experimental determination of the BaO:Fe2O3:TiO2 phase diagram are reported here. All three phases crystallize in space group C2/m (No. 12). Ba2Fe2Ti4O13 (“2:1:4”) is isostructural with K2Ti6O13 and Ba2ZnTi5O13: a=15.1939(9), b=3.8912(3), c=9.1244(5) Å, β=98.456(5)°; Z=2, ρcalc=4.890 g/cc. Ba3Fe10TiO20 (“3:5:1”) is structurally analogous to its aluminum congener Ba3Al10TiO20: a=15.336(1), b=11.7986(9), c=5.1700(4) Å, β=91.220(6)° (I2/m setting); Z=2, ρcalc=4.750 g/cc. Ba4Fe2Ti10O27 (“4:1:10”) is also isostructural with its aluminum analog Ba4Al2Ti10O27: a=19.799(1), b=11.4324(6), c=9.8936(6) Å, β=109.146(4)° (C2/m); Z=4, ρcalc=4.934 g/cc. The 2:1:4 and 3:5:1 compounds adopt open-framework type structures while the 4:1:10 phase exhibits an eight-layer close-packed arrangement.


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