Large-scale synthesis of functional tungsten oxide with controlled oxygen-deficiency by a continuous screw reactor

2021 ◽  
Author(s):  
Eri Kumai ◽  
Fuyumi Shimono ◽  
Manabu Tanaka ◽  
Takayuki Watanabe ◽  
Takeshi Hoshino ◽  
...  
Keyword(s):  
Tungsten Oxide ◽  
Large Scale ◽  
Oxygen Deficiency ◽  
Screw Reactor ◽  
Large Scale Synthesis

Large-Scale Synthesis of Tungsten Oxide Nanowires with High Aspect Ratio

2003 ◽  
Vol 42 (3) ◽  
pp. 921-924 ◽  
Author(s):  
Xiao-Lin Li ◽  
Jun-Feng Liu ◽  
Ya-Dong Li
Keyword(s):  
Aspect Ratio ◽  
Tungsten Oxide ◽  
High Aspect Ratio ◽  
Large Scale ◽  
Oxide Nanowires ◽  
Large Scale Synthesis

scholarly journals Large-Scale Synthesis of Tungsten Oxide (WO3) Nanoleaves, Nanoparticles and Nanoflakes

2013 ◽  
Vol 19 (S2) ◽  
pp. 1580-1581 ◽  
Author(s):  
M. Ahmadi ◽  
M. Guinel
Keyword(s):  
Tungsten Oxide ◽  
Large Scale ◽  
Large Scale Synthesis

Extended abstract of a paper presented at Microscopy and Microanalysis 2013 in Indianapolis, Indiana, USA, August 4 – August 8, 2013.

Large-scale synthesis of tungsten oxide nanofibers by electrospinning

2006 ◽  
Vol 298 (2) ◽  
pp. 996-999 ◽  
Author(s):  
Xiaofeng Lu ◽  
Xincai Liu ◽  
Wanjin Zhang ◽  
Ce Wang ◽  
Yen Wei
Keyword(s):  
Tungsten Oxide ◽  
Large Scale ◽  
Large Scale Synthesis

Exogenous Directing Group Free, Ligand-Enabled gamma-C(sp3)–H Arylation of Free Primary Aliphatic Amines and α-Amino Esters

2019 ◽  
Author(s):  
Yongzheng Ding ◽  
Shuai Fan ◽  
Xiaoxi Chen ◽  
yuzhen gao ◽  
Gang Li
Keyword(s):  
Amino Acids ◽  
Large Scale ◽  
Free Ligand ◽  
Aliphatic Amines ◽  
Rapid Synthesis ◽  
Amino Esters ◽  
Directing Group ◽  
Large Scale Synthesis ◽  
Primary Aliphatic Amines

A Pdᴵᴵ-catalyzed, ligand-enabled gamma-C(sp3)–H arylation of free primary aliphatic amines and amino esters without using an exogenous directing group is reported. This reaction is compatible with unhindered free aliphatic amines, and it is also be applicable to the rapid synthesis of biologically and synthetically valuable unnatural α-amino acids. Large scale synthesis is also feasible using this method.<br>

A Simplified Protocol for the ortho-Deuteration of Acidic Aromatic Compounds in D2O

2019 ◽  
Author(s):  
Alyssa Garreau ◽  
Hanyang Zhou ◽  
Michael Young
Keyword(s):  
Carboxylic Acid ◽  
Aromatic Compounds ◽  
Large Scale ◽  
Simplified Approach ◽  
Directing Group ◽  
Large Scale Synthesis

<div>Methods to catalytically introduce deuterium in synthetically useful yields ortho to a carboxylic acid directing group on arenes typically requires D2 or CD3CO2D, which makes using these approaches cost prohibitive for large scale synthesis (equipment and reagent costs respectively). Herein we present a simplified approach using catalytic RhIII and D2O as deuterium source, and show its application to H/D exchange on various acidic substrates.</div>

A Simplified Protocol for the ortho-Deuteration of Acidic Aromatic Compounds in D2O

2019 ◽  
Author(s):  
Alyssa Garreau ◽  
Hanyang Zhou ◽  
Michael Young
Keyword(s):  
Carboxylic Acid ◽  
Aromatic Compounds ◽  
Large Scale ◽  
Simplified Approach ◽  
Directing Group ◽  
Large Scale Synthesis

<div>Methods to catalytically introduce deuterium in synthetically useful yields ortho to a carboxylic acid directing group on arenes typically requires D2 or CD3CO2D, which makes using these approaches cost prohibitive for large scale synthesis (equipment and reagent costs respectively). Herein we present a simplified approach using catalytic RhIII and D2O as deuterium source, and show its application to H/D exchange on various acidic substrates.</div>

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