Decisive influence of critical process parameters on the microstructure and tensile properties of friction stir back extruded magnesium alloy tubes

2022 ◽  
Vol 73 ◽  
pp. 207-219
Author(s):  
A.K. Lakshminarayanan ◽  
S. Ramachandran ◽  
B. Rajabharathi ◽  
W. Mirihanage
2020 ◽  
Author(s):  
Maria Mendes ◽  
João Basso ◽  
João Sousa ◽  
Alberto Pais ◽  
Carla Vitorino

2019 ◽  
Vol 18 (1) ◽  
pp. 103-111 ◽  
Author(s):  
Sayani Bhattacharyya ◽  
Bharani S Sogali

In the present study custom screening design was employed to observe the effect of four critical process parameters on particle size and polydispersity index of the liposomal formulation made by ethanol injection method. The four process parameters selected were lipid ratio, rate of injection, phase volume ratio and rotational speed of magnetic stirring. Eight different liposomal formulations were prepared using the design. The formulations were subjected to particle size analysis. The analysis was done at a significance level p<0.05 and found that the process parameters had significant effect on the particle size and polydispersity index of the formulations. The design was optimized for the individual responses with an overall desirability of more than 50%. Three batches of liposomes were formulated at optimized process parameters which matched the target as predicted by the design. Therefore, it can be concluded that the design was effective in production of nano sized stable monodisperse liposomes by ethanol injection method. Dhaka Univ. J. Pharm. Sci. 18(1): 103-111, 2019 (June)


Author(s):  
Thomas Robinson ◽  
Malcolm Williams ◽  
Harish Rao ◽  
Ryan P. Kinser ◽  
Paul Allison ◽  
...  

Abstract In recent years, additive manufacturing (AM) has gained prominence in rapid prototyping and production of structural components with complex geometries. Magnesium alloys, whose strength-to-weight ratio is superior compared to steel and aluminum alloys, have shown potential in lightweighting applications. However, commercial beam-based AM technologies have limited success with magnesium alloys due to vaporization and hot cracking. Therefore, as an alternative approach, we propose the use of a near net-shape solid-state additive manufacturing process, Additive Friction Stir Deposition (AFSD), to fabricate magnesium alloys in bulk. In this study, a parametric investigation was performed to quantify the effect of process parameters on AFSD build quality including volumetric defects and surface quality in magnesium alloy AZ31B. In order to understand the effect of the AFSD process on structural integrity in the magnesium alloy AZ31B, in-depth microstructure and mechanical property characterization was conducted on a bulk AFSD build fabricated with a set of acceptable process parameters. Results of the microstructure analysis of the as-deposited AFSD build revealed bulk microstructure similar to wrought magnesium alloy AZ31 plate. Additionally, similar hardness measurements were found in AFSD build compared to control wrought specimens. While tensile test results of the as-deposited AFSD build exhibited a 20 percent drop in yield strength, nearly identical ultimate strength was observed compared to the wrought control. The experimental results of this study illustrate the potential of using the AFSD process to additively manufacture Mg alloys for load bearing structural components with achieving wrought-like microstructure and mechanical properties.


Author(s):  
Tanja A. Grein ◽  
Daniel Loewe ◽  
Hauke Dieken ◽  
Tobias Weidner ◽  
Denise Salzig ◽  
...  

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